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CAS No.: | 112-35-6 |
---|---|
Name: | TRIETHYLENE GLYCOL MONOMETHYL ETHER |
Article Data: | 19 |
Molecular Structure: | |
Formula: | C7H16O4 |
Molecular Weight: | 164.202 |
Synonyms: | 2-[2-(2-Methoxyethoxy)ethoxy]ethanol;3,6,9-Trioxa-1-decanol;3,6,9-Trioxadecanol;Bikanol M 3;Dowanol TMAT;HymolTM;Methyltriglycol;Methyltrioxitol;NSC 97395;Triglycol monomethyl ether; |
EINECS: | 203-962-1 |
Density: | 1.021 g/cm3 |
Melting Point: | -44oC |
Boiling Point: | 233.9 °C at 760 mmHg |
Flash Point: | 95.3 °C |
Solubility: | Completely miscible in water |
Appearance: | Colorless odorless liquid |
Safety: | 24/25-22 |
PSA: | 47.92000 |
LogP: | -0.34170 |
3-Hydroxybenzyl alcohol
A
triethylene glucol monomethyl ether
B
3-Phenoxybenzyl alcohol
Conditions | Yield |
---|---|
A n/a B 87% |
dimethyl sulfate
2,2'-[1,2-ethanediylbis(oxy)]bisethanol
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
With sodium hydroxide at 120℃; for 4h; | 59% |
With sodium hydroxide at 120℃; |
triethylene glycol benzyl methyl ether
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
With hydrogen; palladium | 97% |
2-[2-(2-methoxyethoxy)etoxy]acetic acid
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
Stage #1: 2-[2-(2-methoxyethoxy)etoxy]acetic acid With chloroformic acid ethyl ester; triethylamine In tetrahydrofuran at 22℃; for 0.333333h; Stage #2: With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 1h; Stage #3: With potassium hydrogensulfate In tetrahydrofuran; ethyl acetate at 22℃; for 24h; | 17% |
A
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
With RG7 In toluene at 25℃; Equilibrium constant; |
dimethyl sulfate
2,2'-[1,2-ethanediylbis(oxy)]bisethanol
A
triethylene glucol monomethyl ether
B
Triethylene glycol dimethyl ether
Conditions | Yield |
---|---|
Stage #1: 2,2'-[1,2-ethanediylbis(oxy)]bisethanol With sodium hydroxide at 55 - 60℃; for 0.166667h; Stage #2: dimethyl sulfate at 55 - 60℃; for 6h; | A 33% B n/a |
Conditions | Yield |
---|---|
With solid alkali In 1,4-dioxane; water | 15% |
Conditions | Yield |
---|---|
With phosphoric acid at 60 - 70℃; | |
With sodium methylate at 60 - 140℃; |
triethylene glycol monobenzyl ether
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NaOH 2: 97 percent / H2 / Pd View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aq. NaOH 2: aq. NaOH 3: 97 percent / H2 / Pd View Scheme |
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