Detail of "13547-70-1"

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CAS Number:
13547-70-1
Name:
2-Butanone,1-chloro-3,3-dimethyl-
Superlist Name:
1-Chloropinacolone
Molecular Structure:
Formula:
C₆H₁₁ClO
Molecular Weight:
134.62
Synonyms:
1-Chloro-3,3-dimethyl-2-butanone;3,3-Dimethyl-2-oxobutyl chloride;Chloromethyl tert-butylketone;tert-Butyl chloromethyl ketone;a-Chloropinacolone;
EINECS:
236-920-6
Density:
0.988 g/cm³
Melting Point:
-13 °C(lit.)
Boiling Point:
171.5 °C at 760 mmHg
Flash Point:
61.8 °C
Appearance:
clear slightly yellow liquid
Hazard Symbols:
T,T+,Xi
Risk Codes:
22-23-36/37/38-26-24
Safety:
26-36-45-38-36/37/39-28A Details
Transport Information:
UN 2810

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Reference

Asymmetric synthesis of activated cyclopropanes catalyzed by cinchonidine as a chiral Bronsted base: All Rights Reserved. Asymmetric synthesis of activated cyclopropanes catalyzed by cinchonidine as a chiral Bronsted base.Chemicals with cas numbers 2700-22-3 and 13547-70-1 also play role. Kojima, Satoshi; Suzuki, Maki; Watanabe, Akito; Ohkata, Katsuo ( Department of Chemistry, Graduate School of Science, Hiroshima University 1-3-1 Kagamiyama, Higashi-Hiroshima 739-8526, Japan). Tetrahedron Letters, 47(51), 9061-9065 (English) 2006 Elsevier Ltd. CODEN: TELEAY. ISSN: 0040-4039. DOCUMENT TYPE: Journal CA Section: 24 (Alicyclic Compounds) Cinchonidine catalyzed the cyclopropanation reaction between chloromethyl ketones and b-substituted methylidenemalononitriles to give trans-cyclopropanes with ￡82% ee. Exptl. evidence suggests that cinchonidine functions as a chiral Bronsted base catalyst in the reaction and hydrogen bonding is essential for inducing high enantioselectivity. .

Fungicidal diaryloxytriazolyl-O,N-acetals and salts: Fungicidal diaryloxytriazolyl-O,N-acetals and salts. Kraemer, Wolfgang; Buechel, Karl H.; Brandes, Wilhelm; Kaspers, Helmut (Bayer A.-G., Ger.). Ger. Offen. DE 2455955 12 Aug 1976, 36 pp.There are some reagents with their cas registry numbers 61251-67-0 and 13547-70-1 are used in this study. (German). (Germany). CODEN: GWXXBX. CLASS: IC: C07D249-02. APPLICATION: DE 74-2455955 27 Nov 1974. DOCUMENT TYPE: Patent CA Section: 28 (Heterocyclic Compounds (More Than One Hetero Atom)) Section cross-reference(s): 5, 23, 25 Triazoles (I; R = H, Br, Cl, MeO, MeSO2NMe; R1 = R2 = H, Br, Cl; Y = CO, CHOH; Z = bond, CH2, O, CO, SO2, MeOCH) with fungicidal activity are prepd. by reaction of 1,2,4-triazole (II) with the appropriate 1-bromo-2-butanones, optionally followed by redn. of the keto group. In addn. to 22 I there were prepd. two 1,2,4-triazol-4-yl and two 1,2,3-triazol-1-yl derivs. Thus, reaction of 45 g II with 76.2 g 4-(4-ClC6H4)C6H4OCHBrCOCMe3 gives after 48 hr in 500 ml refluxing MeCN 52.8 g (72%) I (R = Cl, R1 = R2 = H, Y = CO, Z = bond). .

Detail of "13547-70-1"

2-Butanone,1-chloro-3,3-dimethyl-

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CAS No.13547-70-1 1-Chloropinacolone

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