Detail of "152305-23-2"

CAS Number:
152305-23-2
Name:
2-Oxazolidinone,4-[(4-aminophenyl)methyl]-, (4S)-
Superlist Name:
(S)-4-(4-Aminobenzyl)-2(1H)-oxazolidinone
Molecular Structure:
Formula:
C₁₀H₁₂N₂O₂
Molecular Weight:
192.22
Synonyms:
2-Oxazolidinone,4-[(4-aminophenyl)methyl]-, (S)-;(4S)-4-(4-Aminobenzyl)-1,3-oxazolidin-2-one;(S)-4-(4-Aminobenzyl)-2-oxazolidinone;
Density:
1.257 g/cm³
Melting Point:
107-111 °C
Boiling Point:
479.7 °C at 760 mmHg
Flash Point:
243.9 °C
Appearance:
white crystalline powder
Hazard Symbols:
Xn
Risk Codes:
22-36/37/38
Safety:
26-36/37 Details
particular:
particular

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Reference

A validated chiral LC method for the enantiomeric separation of Zolmitriptan key intermediate, ZTR-5: A validated chiral LC method for the enantiomeric separation of Zolmitriptan key intermediate, ZTR-5. Srinivasu, M. K.; Rao, B. Mallikarjuna; Sridhar, G.; Chandrasekhar, K. B.; Kumar, P. Rajender (Analytical Research, Custom Pharmaceutical Services, Dr. Reddy's Laboratories, Hyderabad 500049, India). Journal of Pharmaceutical and Biomedical Analysis, 39(3-4), 796-800 (English) 2005 Elsevier B.V. CODEN: JPBADA. ISSN: 0731-7085. DOCUMENT TYPE: Journal CA Section: 64 (Pharmaceutical Analysis) A new and accurate chiral liq. chromatog. method was described for the enantiomeric sepn. of ZTR-5 [(4S)-4-(4-aminobenzyl)-2-oxazolidinone, (S)-isomer], a key intermediate of Zolmitriptan in bulk drugs. The enantiomers of ZTR-5 were baseline resolved on a Chiralpak AD-H (250 mm ′ 4.6 mm, 5 mm) column using a mobile phase system contg. hexane:ethanol (, vol./vol.). The resoln. between the enantiomers was not less than 4 and interestingly distomer was eluted prior to eutomer. The limit of detection and limit of quantification of (4R)-4-(4-aminobenzyl)-2-oxazolidinone [(R)-isomer] were found to be 250 and 750 ng/mL, resp. There are some commonly used reagents like 152305-23-2 in this article., for 10 mL injection vol.In this study，152305-23-2 is also used. The percentage recovery of (R)-isomer ranged from 92.0 to 105.6 in the bulk drug samples of ZTR-5. The validated method yielded good results regarding precision, linearity, accuracy, and ruggedness. The proposed method was found to be suitable and accurate for the quant. detn. of (R)-isomer in bulk drug samples of ZTR-5. ..

A validated chiral LC method for the enantiomeric separation of Zolmitriptan key intermediate, ZTR-5: A validated chiral LC method for the enantiomeric separation of Zolmitriptan key intermediate, ZTR-5. Srinivasu, M. K.; Rao, B. Mallikarjuna; Sridhar, G.; Chandrasekhar, K. B.; Kumar, P. Rajender (Analytical Research, Custom Pharmaceutical Services, Dr. Reddy's Laboratories, Hyderabad 500049, India). Journal of Pharmaceutical and Biomedical Analysis, 39(3-4), 796-800 (English) 2005 Elsevier B.V. CODEN: JPBADA. ISSN: 0731-7085. DOCUMENT TYPE: Journal CA Section: 64 (Pharmaceutical Analysis) A new and accurate chiral liq. chromatog. method was described for the enantiomeric sepn. of ZTR-5 [(4S)-4-(4-aminobenzyl)-2-oxazolidinone, (S)-isomer], a key intermediate of Zolmitriptan in bulk drugs. The enantiomers of ZTR-5 were baseline resolved on a Chiralpak AD-H (250 mm ′ 4.6 mm, 5 mm) column using a mobile phase system contg. hexane:ethanol (, vol./vol.). The resoln. between the enantiomers was not less than 4 and interestingly distomer was eluted prior to eutomer. The limit of detection and limit of quantification of (4R)-4-(4-aminobenzyl)-2-oxazolidinone [(R)-isomer] were found to be 250 and 750 ng/mL, resp. There are some commonly used reagents like 152305-23-2 in this article., for 10 mL injection vol.In this study，152305-23-2 is also used. The percentage recovery of (R)-isomer ranged from 92.0 to 105.6 in the bulk drug samples of ZTR-5. The validated method yielded good results regarding precision, linearity, accuracy, and ruggedness. The proposed method was found to be suitable and accurate for the quant. detn. of (R)-isomer in bulk drug samples of ZTR-5. ..

Detail of "152305-23-2"

2-Oxazolidinone,4-[(4-aminophenyl)methyl]-, (4S)-

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Reference