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172152-35-1

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CAS No.: 172152-35-1
Name: 2-[[(4-Methoxy-3-methyl-2-pyridinyl)methyl]thio]-6-(1H-pyrrol-1-yl)-1H-benzimidazole
Article Data: 5
Molecular Structure:
Molecular Structure of 172152-35-1 (2-[[(4-Methoxy-3-methyl-2-pyridinyl)methyl]thio]-6-(1H-pyrrol-1-yl)-1H-benzimidazole)
Formula: C19H18N4OS
Molecular Weight: 350.444
Synonyms: 2-[[(4-Methoxy-3-methyl-2-pyridinyl)methyl]thio]-6-(1H-pyrrol-1-yl)-1H-benzimidazole;5-(1H-pyrrol-1-yl)-2-[(4-methoxy-3-methyl-2-pyridyl)-methylthio]-1-hydro-benzimidazole
Density: 1.30±0.1 g/cm3(Predicted)
Boiling Point: 590.4±60.0 °C(Predicted)
PSA: 81.03000
LogP: 4.35790
Related products
Synthetic route
172152-53-3

5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole-2-thiol

86604-74-2

2-chloromethyl-4-methoxy-3-methylpyridine hydrochloride

172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

Conditions
ConditionsYield
With sodium hydroxide at 40℃; Solvent; Reagent/catalyst;89.7%
With sodium hydroxide In methanol at 50℃; for 1.5h;81.2%
696-59-3

cis,trans-2,5-dimethoxytetrahydrofuran

910664-00-5

5-amino-2-[(4-methoxy-3-methyl-2-pyridyl)-methylthio]-1-hydro-benzimidazole

172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

Conditions
ConditionsYield
With acetic acid at 120℃; for 0.0833333h;38.1%
With acetic acid for 0.0833333h; Product distribution / selectivity; Heating / reflux;
172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)sulfinyl)-5-(1H-pyrrol-1-yl)benzimidazol-1-ide sodium salt

Conditions
ConditionsYield
With sodium hypochlorite; sodium hydroxide In tetrahydrofuran; water at 0 - 5℃; for 1.5h; Solvent;94.7%
172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

834897-64-2

ilaprazole

Conditions
ConditionsYield
With peracetic acid; sodium tungstate; C94H124N6 In water at 0℃; for 8h; Inert atmosphere;90%
172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

910664-01-6

ilaprazole

Conditions
ConditionsYield
With sodium molybdate; C78H60Cl8N6; dihydrogen peroxide In water at 0℃; for 8h; Inert atmosphere;90%
172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

ilaprazole

Conditions
ConditionsYield
With tert.-butylnitrite; dihydrogen peroxide In tert-butyl alcohol at 0 - 25℃; for 10h;83%
Stage #1: 2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole With triethylamine In ethanol at 30℃; for 0.166667h; pH=8-9;
Stage #2: With dihydrogen peroxide In ethanol for 6h; Reagent/catalyst;		75%
With 3-chloro-benzenecarboperoxoic acid In chloroform at -40℃; for 0.333333h;64%
With 3-chloro-benzenecarboperoxoic acid In chloroform at 20℃;45.5%
With NADPH; cytochrome P450 In aq. phosphate buffer at 37℃; for 0.75h; pH=7.4; Enzymatic reaction;
172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

(-)-5-(1H-pyrrol-1-yl)-2-[[(4-methoxy-3-methyl-2-pyridyl)-methyl]sulfinyl]-1-hydro-benzimidazole

Conditions
ConditionsYield
With titanium(IV) isopropylate; tert.-butylhydroperoxide; water; (R)-1,1'-Bi-2-naphthol; N-ethyl-N,N-diisopropylamine In toluene at 25℃; for 16h; Product distribution / selectivity;60.9%
With titanium(IV) isopropylate; L-(+)-diisopropyl tartrate; Cumene hydroperoxide; water; N-ethyl-N,N-diisopropylamine In toluene at 25 - 30℃; for 3.5 - 5.5h; Product distribution / selectivity;55.3%
With titanium(IV) isopropylate; Cumene hydroperoxide; water; (R)-1,1'-Bi-2-naphthol; N-ethyl-N,N-diisopropylamine In toluene at 25℃; for 13h; Product distribution / selectivity;53.2%
172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

(-)-5-(1H-pyrrol-1-yl)-2-[[(4-methoxy-3-methyl-2-pyridyl)-methyl]sulfinyl]-1-hydro-benzimidazole

Conditions
ConditionsYield
Stage #1: 2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole With titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In chloroform at 20 - 31℃; for 1h;
Stage #2: With Cumene hydroperoxide; N-ethyl-N,N-diisopropylamine In chloroform at 31℃; for 18h; Product distribution / selectivity;		49.7%
Stage #1: 2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole With titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In chloroform at 20 - 31℃; for 1h;
Stage #2: With Cumene hydroperoxide; N-ethyl-N,N-diisopropylamine In chloroform at 31℃; for 18h; Product distribution / selectivity;		49.7%
Stage #1: 2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole With titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In chloroform at 20 - 80℃; for 0.0833333h; Molecular sieve;
Stage #2: With water In chloroform at 20 - 80℃; for 1h; Molecular sieve;
Stage #3: With Cumene hydroperoxide; N-ethyl-N,N-diisopropylamine In chloroform at 20 - 80℃; for 16 - 18h; Product distribution / selectivity; Molecular sieve;		35.5%
172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

(-)-5-(1H-pyrrol-1-yl)-2-[[(4-methoxy-3-methyl-2-pyridyl)-methyl]sulfinyl]-1-hydro-benzimidazole

(-)-5-(1H-pyrrol-1-yl)-2-[[(4-methoxy-3-methyl-2-pyridyl)-methyl]sulfinyl]-1-hydro-benzimidazole

Conditions
ConditionsYield
Stage #1: 2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole With titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In dichloromethane for 0.0833333h;
Stage #2: With Cumene hydroperoxide; N-ethyl-N,N-diisopropylamine In dichloromethane; water at 20℃; for 22h; Product distribution / selectivity;		A n/a
B 37.7%
Stage #1: 2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole With titanium(IV) isopropylate; diethyl (2S,3S)-tartrate In chloroform for 0.0833333h;
Stage #2: With Cumene hydroperoxide; N-ethyl-N,N-diisopropylamine In chloroform; water at 20 - 30℃; for 1 - 18h; Product distribution / selectivity;		A n/a
B 32.7%
Stage #1: 2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole With titanium(IV) isopropylate; diethyl (2S,3S)-tartrate; 4 A molecular sieve In toluene
Stage #2: With Cumene hydroperoxide; N-ethyl-N,N-diisopropylamine In water; toluene
Stage #3: With Cumene hydroperoxide; N-ethyl-N,N-diisopropylamine In chloroform at 20 - 30℃; for 1 - 18h; Product distribution / selectivity;		A n/a
B 32.7%
172152-35-1

2-(((4-methoxy-3-methylpyridin-2-yl)methyl)thio)-5-(1H-pyrrol-1-yl)-1H-benzo[d]imidazole

5-(1H-pyrrol-1-yl)-2-[[(4-methoxy-3-methyl)-2-pyridyl-1-oxide]methyl]sulfinyl-1H-benzimidazole

Conditions
ConditionsYield
With dihydrogen peroxide; acetic acid In methanol at 45℃;3.58 g
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    instock with good quality and wholesale price Storage:Keep in a cool & dry place Package:Packing material and QTY as your request Application:Pharma;Industry;other application Transportation:Express or as your request Port:Any port of China

    Wuhan MoonZY Biological Technology Co.,Ltd (MoonzyBio)is located in Wuhan city,hubei province,China,we have a group of senior technical backbones, specialized in R & D and sales in

  • Wuhan MoonZY Biological Technology Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:13545198479

    Address:203,Building 3, International Enterprise Center, No. 1 Guanshan 2nd Road, East Lake New Technology Development Zone,

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  • 2-[[(4-Methoxy-3-methyl-2-pyridinyl)methyl]thio]-6-(1H-pyrrol-1-yl)-1H-benzimidazole

  • Casno:

    172152-35-1

    2-[[(4-Methoxy-3-methyl-2-pyridinyl)methyl]thio]-6-(1H-pyrrol-1-yl)-1H-benzimidazole

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por

    Shanghai fine pharma co., Ltd. is a professional enterprise with chemical reagents and fine chemical products development, development and trade. The company has a sound research a

  • Shanghai Run-Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-21-31576854/57171705 / 57171706

    Address:second floor, building 3, No.999, jiangyue Road, minghang District, Shanghai, China

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  • TIANFU 2-[[(4-Methoxy-3-methyl-2-pyridinyl)methyl]thio]-6-(1H-pyrrol-1-yl)-1H-benzimidazole

  • Casno:

    172152-35-1

    TIANFU 2-[[(4-Methoxy-3-methyl-2-pyridinyl)methyl]thio]-6-(1H-pyrrol-1-yl)-1H-benzimidazole

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

    Our company has been engaged in the Pharmaceutical raw material and pharmaceutical intermediates medicine material intermediates and related chemical industry for more than ten ye

  • Taizhou volsen chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-576-88869393

    Address:Jiaojiang District, Taizhou, Zhejiang, China.

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  • 172152-35-1

  • Casno:

    172152-35-1

    172152-35-1

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    TIANFU 2-[[(4-Methoxy-3-methyl-2-pyridinyl)methyl]thio]-6-(1H-pyrrol-1-yl)-1H-benzimidazole Application:Intermediates

    We are Hebei minshang biotechnology co. LTD., mainly deal in pharmaceutical intermediates and various chemicals. We are manufacturers and have our own factory. Products & Usage Ph

  • Hebei Minshang Biotechnology Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:18032092709

    Address:hebei

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