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Basic Information
| CAS No.: | 205687-01-0 |
|---|---|
| Name: | Capsiate |
| Article Data: | 6 |
| Molecular Structure: | |
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| Formula: | C18H26O4 |
| Molecular Weight: | 306.402 |
| Synonyms: | Capsiate Natura;UNII-PX8I7HG5I3;capsiate; |
| Density: | 1.053 |
| Boiling Point: | 421.3±40.0 °C(Predicted) |
| PSA: | 55.76000 |
| LogP: | 4.21660 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| Novozym 435 at 50℃; for 16h; Polyacrylate; | 86.6% |
| With di-isopropyl azodicarboxylate; thiamine diphosphate In tetrahydrofuran at 20℃; Mitsunobu esterification; | 51% |
- 1073340-78-9
4-t-butyldimethylsilyloxy-3-methoxybenzyl (E)-8-methylnon-6-enoate
- 205687-01-0
capsiate
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; water In ethanol at 20℃; for 18h; Inert atmosphere; | 79.42% |
- 5129-54-4
8-methylnonanoic acid methyl ester
- 5129-53-3
methyl isononanoate
- 498-00-0
4-hydroxymethyl-2-methoxyphenol
- 112375-54-9
(E)-methyl 8-methyl-6-nonenoate
B
- 205687-01-0
capsiate
Conditions
| Conditions | Yield |
|---|---|
| novozyme 435 at 25℃; for 45h; |
...Expand
- 59320-77-3
trans-8-methyl-6-nonenoic acid
- 205687-01-0
capsiate
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: thionyl chloride / 1 h / 60 °C 2: pyridine / 18 h / Inert atmosphere 3: hydrogenchloride; water / ethanol / 18 h / 20 °C / Inert atmosphere View Scheme |
- 69404-94-0
O-tert-butyldimethylsilylvanillin
- 205687-01-0
capsiate
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 48 h / 20 °C / Cooling with ice; Inert atmosphere 2: pyridine / 18 h / Inert atmosphere 3: hydrogenchloride; water / ethanol / 18 h / 20 °C / Inert atmosphere View Scheme |
- 121-33-5
vanillin
- 205687-01-0
capsiate
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1: pyridine / 24 h / 20 °C / Inert atmosphere 2: diisobutylaluminium hydride / tetrahydrofuran; toluene / 48 h / 20 °C / Cooling with ice; Inert atmosphere 3: pyridine / 18 h / Inert atmosphere 4: hydrogenchloride; water / ethanol / 18 h / 20 °C / Inert atmosphere View Scheme |
- 31467-60-4
(6Z)-8-methyl-6-nonaneneoic acid
- 205687-01-0
capsiate
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1: nitric acid; sodium nitrite / water / 1.5 h / 70 °C / Inert atmosphere 2: thionyl chloride / 1 h / 60 °C 3: pyridine / 18 h / Inert atmosphere 4: hydrogenchloride; water / ethanol / 18 h / 20 °C / Inert atmosphere View Scheme |
- 95636-02-5
(E)-8-Methylnon-6-enoic acid chloride
- 113931-96-7
4-<(tert-butyldimethylsilyl)oxy>-3-methoxybenzyl alcohol
- 205687-01-0
capsiate
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: pyridine / 18 h / Inert atmosphere 2: hydrogenchloride; water / ethanol / 18 h / 20 °C / Inert atmosphere View Scheme |
- 3947-62-4, 6207-76-7, 19235-21-3, 22554-70-7, 22860-22-6, 47339-09-3, 57884-82-9, 62057-79-8, 70191-05-8, 109525-54-4, 140147-37-1, 10343-06-3
2,3,4,5-tetra-O-acetyl-D-glucopyranose
- 205687-01-0
capsiate
Conditions
| Conditions | Yield |
|---|---|
| With triphenylphosphine; diethylazodicarboxylate In toluene at 20℃; for 17h; Cooling with ice; Overall yield = 67 %; Overall yield = 4.58 g; | A n/a B n/a |
...Expand
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