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Basic Information
CAS No.: 2459-09-8
Name: Methyl isonicotinate
Article Data: 96
Molecular Structure:
Molecular Structure of 2459-09-8 (Methyl isonicotinate)
Formula: C7H7NO2
Molecular Weight: 137.138
Synonyms: Isonicotinicacid, methyl ester (6CI,7CI,8CI);4-Carbomethoxypyridine;4-Methoxycarbonylpyridine;Methyl 4-pyridinecarboxylate;4-Pyridinecarboxylicacid, methyl ester;
EINECS: 219-546-8
Density: 1.137 g/cm3
Melting Point: 8-8.5 °C(lit.)
Boiling Point: 205.1 °C at 760 mmHg
Flash Point: 77.8 °C
Solubility: Slightly soluble in water.
Appearance: clear orange to brown liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
PSA: 39.19000
LogP: 0.86820
Synthetic route
3783-38-8

methyl isonicotinate N-oxide

2459-09-8

4-pyridinecarboxylic acid, methyl ester

Conditions
ConditionsYield
With ammonium formate; palladium on activated charcoal In methanol for 0.0166667h; Ambient temperature;98%
With sodium hypophosphite; palladium on activated charcoal In acetic acid at 60℃; for 1h;98%
With ammonium formate; silica gel; zinc In methanol at 20℃; for 0.166667h; chemoselective reaction;97%
872-85-5

pyridine-4-carbaldehyde

67-56-1

methanol

2459-09-8

4-pyridinecarboxylic acid, methyl ester

Conditions
ConditionsYield
With water; iodine; sodium nitrite at 20 - 70℃; chemoselective reaction;96%
With potassium carbonate In water at 20℃; for 2h;89%
With dibromamine-T; potassium carbonate at 20℃; for 1h;83%
55-22-1

pyridine-4-carboxylic acid

67-56-1

methanol

2459-09-8

4-pyridinecarboxylic acid, methyl ester

Conditions
ConditionsYield
With sulfuric acid for 24h; Heating;95%
With sulfuric acid for 72h; Reflux;92%
With sulfuric acid Reflux;80%
67-56-1

methanol

1570-45-2

isonicotinic acid ethylester

2459-09-8

4-pyridinecarboxylic acid, methyl ester

Conditions
ConditionsYield
With lanthanum complex grafted upon hydrotalcite for 4h; pH=10; Reflux;95%
67-56-1

methanol

25108-37-6

potassium pyridine-4-carboxylate

2459-09-8

4-pyridinecarboxylic acid, methyl ester

Conditions
ConditionsYield
With tetrachloromethane; triphenylphosphine at 55 - 60℃;91%
626-61-9

4-Chloropyridine

67-56-1

methanol

201230-82-2

carbon monoxide

865-34-9

lithium methanolate

2459-09-8

4-pyridinecarboxylic acid, methyl ester

Conditions
ConditionsYield
With 1,1'-bis-(diphenylphosphino)ferrocene; 5 mol% Pd/C; sodium fluoride In 1,4-dioxane at 150℃; Inert atmosphere;88%
55-22-1

pyridine-4-carboxylic acid

74-88-4

methyl iodide

2459-09-8

4-pyridinecarboxylic acid, methyl ester

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide at 20℃; for 0.5h;85%
108-89-4

picoline

67-56-1

methanol

A

2459-09-8

4-pyridinecarboxylic acid, methyl ester

B

22796-40-3

4-trichloromethyl-pyridine

Conditions
ConditionsYield
Stage #1: picoline With thionyl chloride for 3h; Reflux;
Stage #2: methanol In water
A 18%
B 82%
67-56-1

methanol

1701-69-5

1-(4-pyridyl)-1-propanone

2459-09-8

4-pyridinecarboxylic acid, methyl ester

Conditions
ConditionsYield
With N,N-dimethyl-formamide dimethyl acetal for 16h; Heating;71%
54-85-3

isoniazid

2459-09-8

4-pyridinecarboxylic acid, methyl ester

Conditions
ConditionsYield
With methanol; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In chloroform at 20℃; for 1h;70%
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Chemistry


IUPAC Name: Methyl pyridine-4-carboxylate
Canonical SMILES: COC(=O)C1=CC=NC=C1
InChI: InChI=1S/C7H7NO2/c1-10-7(9)6-2-4-8-5-3-6/h2-5H,1H3
InChIKey: OLXYLDUSSBULGU-UHFFFAOYSA-N
Molecular Weight: 137.13598 [g/mol]
Molecular Formula: C7H7NO2
XLogP3: 0.9
H-Bond Donor: 0
H-Bond Acceptor: 3 
EINECS: 219-546-8 
storage temp. 2-8 °C
Appearance: clear orange to brown liquid
Melting Point: 8-8.5 °C(lit.)
Index of Refraction: 1.511
Molar Refractivity: 36.11 cm3
Molar Volume: 120.5 cm3
Surface Tension: 41.6 dyne/cm
Density: 1.137 g/cm3
Flash Point: 77.8 °C
Enthalpy of Vaporization: 44.13 kJ/mol
Boiling Point: 205.1 °C at 760 mmHg
Vapour Pressure: 0.255 mmHg at 25 °C 
Product Categories of Methyl isonicotinate (CAS NO.2459-09-8): C7 and C8; Heterocyclic Building Blocks; Pyridines

Uses

 Methyl isonicotinate (CAS NO.2459-09-8) is used for pharmaceutical intermediates.

Safety Profile

Hazard Codes: IrritantXi
Risk Statements: 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36:Wear suitable protective clothing.
WGK Germany: 3
F: 10
Hazard Note of Methyl isonicotinate (CAS NO.2459-09-8): Irritant

Specification

 Methyl isonicotinate (CAS NO.2459-09-8), its Synonyms are 4-Methoxycarbonylpyridine ; Isonicotinic acid methyl ester ; Methyl 4-pyridinecarboxylate ; N-Methylisonicotinate ; Isonicotinic acid, methyl ester (8CI) .