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30556-86-6

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Basic Information
CAS No.: 30556-86-6
Name: 3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctylamine
Article Data: 14
Molecular Structure:
Molecular Structure of 30556-86-6 (3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctylamine)
Formula: C8H6F13N
Molecular Weight: 363.122
Synonyms: 1-Octanamine,3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro;3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctylamine;1H,1H,2H,2H-perfluorooctylamine;
PSA: 26.02000
LogP: 4.77430
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Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In diethyl ether at 20℃; under 5171.62 Torr;88%
With hydrazine hydrate; nickel In water at 60℃; for 8h;83%
With lithium aluminium tetrahydride In tetrahydrofuran77%
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Conditions
ConditionsYield
With sodium azide; N2H4*H2O-Raney Ni; hydrazine hydrate Multistep reaction;
Multi-step reaction with 2 steps
1: sodium azide; Aliquot 336 / H2O / Heating
2: H2 / Pd/C / diethyl ether / 2585.74 Torr
View Scheme
Multi-step reaction with 2 steps
1: NaN3 / dimethylformamide / 72 h / 20 °C
2: 8.1 g / H2 / Pd/C / diethyl ether / 12 h / 5250.42 Torr
View Scheme
30556-86-6

3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctylamine

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acryloyl chloride

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Conditions
ConditionsYield
With triethylamine In chloroform Solvent; Concentration; Cooling with ice;99%
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isocyanate de chloro-4 phenoxysulfonyle

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3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctylamine

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Conditions
ConditionsYield
In toluene at 0℃; for 0.0833333h; Addition;98%
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3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctylamine

(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluoro-octyl)-[2-[(E)-3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octylimino]-eth-(E)-ylidene]-amine

Conditions
ConditionsYield
In methanol at 20℃; for 48h; Condensation;98%
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Isopropyl isocyanate

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Conditions
ConditionsYield
In dichloromethane at 20℃; for 0.5h;95%
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3-Hydroxy-2-hydroxymethyl-2-methyl-N-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-propionamide

Conditions
ConditionsYield
With tertiary amine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate94%
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3-(tert-butyloxycarbonylamino)propionic acid

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C16H19F13N2O3

Conditions
ConditionsYield
Stage #1: 3-(tert-butyloxycarbonylamino)propionic acid With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.166667h;
Stage #2: 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctylamine In dichloromethane at 20℃; for 12h;		94%
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epichlorohydrin

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Conditions
ConditionsYield
at 40 - 45℃; for 15h;93%
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3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctylamine

[(S)-1,2-Bis-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane92%
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine In acetonitrile for 3h; Ambient temperature;66%
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