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32360-03-5

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Basic Information
CAS No.: 32360-03-5
Name: 2-tert-Butyl-5-pentadecylphenol
Article Data: 3
Molecular Structure:
Molecular Structure of 32360-03-5 (2-tert-Butyl-5-pentadecylphenol)
Formula: C25H44O
Molecular Weight: 360.624
Synonyms: 3-n-pentadecyl-2-tert-butylphenol;2-tert-butyl-5-n-pentadecylphenol;5-pentadecyl-2-tert-butyl-phenol;
Density: 0.897g/cm3
Melting Point: 43.5 °C(Solv: chloroform (67-66-3); hexane (110-54-3))
Boiling Point: 458.4°Cat760mmHg
Flash Point: 216.2°C
PSA: 20.23000
LogP: 8.32340
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Synthetic route
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tert-butyl methyl ether

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3-n-Pentadecylphenol

32360-03-5

2-tert-butyl-5-n-pentadecylphenol

Conditions
ConditionsYield
tin(IV) chloride In dichloromethane for 16h; Ambient temperature;98%
507-20-0

tertiary butyl chloride

501-24-6

3-n-Pentadecylphenol

32360-03-5

2-tert-butyl-5-n-pentadecylphenol

Conditions
ConditionsYield
With zinc(II) chloride In acetone at 60℃; for 3h; Temperature;
With zinc(II) chloride In acetone at 50℃; for 5h;31.2 g
32360-03-5

2-tert-butyl-5-n-pentadecylphenol

106-93-4

ethylene dibromide

2-(2-bromo-ethoxy)-1-tert-butyl-4-pentadecyl-benzene

Conditions
ConditionsYield
With potassium hydroxide at 70℃; for 6h;88%
32360-03-5

2-tert-butyl-5-n-pentadecylphenol

106-95-6

allyl bromide

502495-06-9

2-allyloxy-1-tert-butyl-4-n-pentadecylbenzene

Conditions
ConditionsYield
With potassium carbonate In acetone Heating;80%
32360-03-5

2-tert-butyl-5-n-pentadecylphenol

4392-24-9

Cinnamyl bromide

1-tert-butyl-4-n-pentadecyl-2-(3-phenylallyloxy)benzene

Conditions
ConditionsYield
With potassium carbonate In acetone Heating;79%
32360-03-5

2-tert-butyl-5-n-pentadecylphenol

3-n-pentadecyl-6-tert-butyl-2,4-dinitrophenol

Conditions
ConditionsYield
With nitric acid In methanol at 20℃; for 0.5h;79%
4784-77-4, 39616-19-8, 29576-14-5

(E)-1-Bromo-2-butene

32360-03-5

2-tert-butyl-5-n-pentadecylphenol

2-(but-2-enyloxy)-1-tert-butyl-4-n-pentadecylbenzene

Conditions
ConditionsYield
With potassium carbonate In acetone Heating;77%
32360-03-5

2-tert-butyl-5-n-pentadecylphenol

265310-65-4

2-tert-butyl-5-n-pentadecyl-1,4-benzoquinone

Conditions
ConditionsYield
With water; dihydrogen peroxide; acetic acid; methyltrioxorhenium(VII) at 25℃; for 12h; Catalytic oxidation;71%
With poly(4-vinylpyridine) 25 percent cross-linked; dihydrogen peroxide; methyltrioxorhenium(VII) In ethanol; water at 40℃;
Multi-step reaction with 2 steps
1: K2CO3 / dimethylformamide / 12 h / 25 °C
2: 49 percent / H2O2; H2O; AcOH / methyltrioxorhenium(VII) / 12 h / 25 °C
View Scheme
32360-03-5

2-tert-butyl-5-n-pentadecylphenol

A

3-n-pentadecyl-6-tert-butyl-2-nitrophenol

B

2-tert-butyl-5-n-pentadecyl-4-nitrophenol

Conditions
ConditionsYield
With nitric acid In methanol at 20℃; for 0.5h;A 15%
B 69%
32360-03-5

2-tert-butyl-5-n-pentadecylphenol

172759-21-6

2-tert-butyl-4-bromo-5-n-pentadecylphenol

Conditions
ConditionsYield
With bromine In tetrachloromethane at 0℃; for 0.25h;
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