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CAS No.: | 4074-90-2 |
---|---|
Name: | ADIPIC ACID DIVINYL ESTER |
Article Data: | 20 |
Molecular Structure: | |
Formula: | C10H14 O4 |
Molecular Weight: | 198.219 |
Synonyms: | Adipicacid, divinyl ester (6CI,7CI,8CI); Hexanedioic acid, diethenyl ester (9CI);Divinyl adipate; Divinyl hexanedioate |
Density: | 1.039g/cm3 |
Melting Point: | 28 °C |
Boiling Point: | 261.1°Cat760mmHg |
Flash Point: | 122.2°C |
Safety: | Low toxicity by ingestion. When heated to decomposition it emits acrid smoke and irritating vapors. |
PSA: | 52.60000 |
LogP: | 1.92020 |
Conditions | Yield |
---|---|
With sulfuric acid; mercury(II) diacetate for 4h; Reflux; Inert atmosphere; | 52% |
With mercury(II) sulfate | |
With sulfuric acid; mercury(II) diacetate; copper diacetate at 70℃; | |
With mercury(II) sulfate |
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether In acetonitrile at 40 - 50℃; for 20h; Inert atmosphere; | 48% |
Conditions | Yield |
---|---|
With trihexyl(tetradecyl)phosphonium chloride; tetrabutyl-ammonium chloride; copper diacetate; tetrahexylammonium chloride; palladium; copper dichloride In 1,4-dioxane for 21h; Catalytic behavior; High pressure; | 16% |
Conditions | Yield |
---|---|
With pyridine |
Conditions | Yield |
---|---|
With chloroacetic acid; mercury(II) oxide at 80℃; | |
rhenium(I) pentacarbonyl chloride In toluene at 140℃; under 15001.5 Torr; for 6h; Product distribution / selectivity; | 96 %Chromat. |
rhenium In toluene at 160℃; under 15001.5 Torr; for 6h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
In xylene for 1h; Heating; |
divinyl adipate
Conditions | Yield |
---|---|
With diisopropylamine In chloroform for 12h; Reflux; | 0.15 g |
Conditions | Yield |
---|---|
With Thermomyces lanuginosus lipase; potassium carbonate In dimethyl sulfoxide at 50℃; for 0.5h; Flow reactor; Enzymatic reaction; | 99% |
With D-aminoacylase from Escherichia coli (EC 3.5.1.81) In dimethyl sulfoxide at 50℃; for 96h; | 95% |
In various solvent(s) at 50℃; for 60h; Markovnikov's addition; | 94% |
divinyl adipate
ribavirin
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; lipase acrylic resin from Candida antartica In acetone at 50℃; for 4h; | 96% |
With [bmim]BF4; Candida antarctica lipase acrylic resin In acetone at 50℃; for 12h; | 98.5 % Chromat. |
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