CAS No.4093-35-0,BROMOPRIDE Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	4093-35-0
Name:	BROMOPRIDE
Article Data:	14

Formula:	C14H22 Br N3 O2
Molecular Weight:	344.252
Synonyms:	o-Anisamide,4-amino-5-bromo-N-[2-(diethylamino)ethyl]- (7CI,8CI); 2-Methoxy-4-amino-5-bromo-N,N-diethylaminoethylbenzamide;Bromopride; Emepride; Emoril;N-Diethylaminoethyl-2-methoxy-4-amino-5-bromobenzamide; Viadil
Density:	1.313g/cm³
Melting Point:	148-150?C
Boiling Point:	435.8°Cat760mmHg
Flash Point:	217.3°C
Hazard Symbols:
Risk Codes:	20/21/22
Safety:	Poison by ingestion and intraperitoneal routes. Experimental reproductive effects. When heated to decomposition it emits toxic fumes of NO_x and Br⁻.
PSA:	67.59000
LogP:	3.08360

Synthetic route

: 201230-82-2
carbon monoxide

: 1285695-16-0
2-bromo-4-iodo-5-methoxyaniline

: 100-36-7
N,N-diethylethylenediamine

: 4093-35-0
bromopride

Conditions

Conditions	Yield
With triethylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane at 80℃; Inert atmosphere; Sealed chamber;	74.7 mg

...Expand

: 5344-78-5
4-bromo-3-nitroanizole

: 4093-35-0
bromopride

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: hydrogenchloride; iron / ethanol; water / 3 h / Reflux 2: tetramethylammonium dichloroiodate(I) / ethyl acetate / 96 h 3: triethylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) / 1,4-dioxane / 80 °C / Inert atmosphere; Sealed chamber View Scheme

: 59557-92-5
2-bromo-5-methoxyaniline

: 4093-35-0
bromopride

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: tetramethylammonium dichloroiodate(I) / ethyl acetate / 96 h 2: triethylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) / 1,4-dioxane / 80 °C / Inert atmosphere; Sealed chamber View Scheme

: 96-96-8
4-methoxy-2-nitroaniline

: 4093-35-0
bromopride

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: sulfuric acid; acetic acid; sodium nitrite / water / 15 - 20 °C 1.2: 20 - 80 °C 2.1: hydrogenchloride; iron / ethanol; water / 3 h / Reflux 3.1: tetramethylammonium dichloroiodate(I) / ethyl acetate / 96 h 4.1: triethylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) / 1,4-dioxane / 80 °C / Inert atmosphere; Sealed chamber View Scheme

: 4093-35-0
bromopride

: Bromoprid-N-oxid

Conditions

Conditions	Yield
With dihydrogen peroxide In ethanol Ambient temperature;	11%

: 4093-35-0
bromopride

: 4-amino-5-bromo-N-(2-diethylamino-ethyl)-3-iodo-2-methoxy-benzamide

Conditions

Conditions	Yield
Stage #1: bromopride With trifluoroacetic acid; thallium(III) trifluoroacetate at 20℃; for 0.5h; thallation; Stage #2: With trifluoroacetic acid; sodium iodide at 20℃; for 5h; Iodination; Further stages.;

: 4093-35-0
bromopride

: [131I]-iodo-Bromopride

Conditions

Conditions	Yield
Stage #1: bromopride With trifluoroacetic acid; thallium(III) trifluoroacetate for 0.166667h; thallation; Stage #2: With [131I]-sodium iodide; trifluoroacetic acid for 0.0833333h; Iodination; Further stages.;

: 4093-35-0
bromopride

: 6203-18-5
p-dimethylaminocinnamaldehyde

: C25H34BrN4O2(1+)

Conditions

Conditions	Yield
With hydrogenchloride; sodium dodecyl-sulfate In water Reagent/catalyst; Flow reactor;

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Chemistry

IUPAC Name: 4-amino-5-bromo-N-(2-diethylaminoethyl)-2-methoxybenzamide
Synonyms: 4-amino-5-bromo-n-(2-(diethylamino)ethyl)-2-methoxy-benzamid ; 4-amino-5-bromo-n-(2-(diethylamino)ethyl)-o-anisamid ; Artomey ; Bromoprida ; Emepride
Product Categories: Intermediates & Fine Chemicals;Pharmaceuticals
Molecular Formula of Valopride (CAS NO. 4093-35-0 ) : C₁₄H₂₂BrN₃O₂
Structure of Valopride (CAS NO.4093-35-0 ) :

EINECS: 223-842-2
Molecular Weight: 344.25 g/mol
Surface Tension: 44.8 dyne/cm
Index of Refraction: 1.565
Melting point : 149°C
Storage temp: 2-8°C
Density: 1.313 g/cm³
Flash Point: 217.3 °C
Boiling Point: 435.8 °C at 760 mmHg
Vapour Pressure: 8.53E-08 mmHg at 25°C
Enthalpy of Vaporization: 69.21 kJ/mol
Appearance: a solid

Uses

Valopride (CAS NO.4093-35-0 ) was used as an antiemetic.

Toxicity Data With Reference

1.	orl-rat LD50:545 mg/kg	YAKUD5 Gekkan Yakuji. Pharmaceuticals Monthly. 21 (1979),516.
2.	ipr-rat LD50:125 mg/kg	YAKUD5 Gekkan Yakuji. Pharmaceuticals Monthly. 21 (1979),516.
3.	orl-mus LD50:310 mg/kg	YAKUD5 Gekkan Yakuji. Pharmaceuticals Monthly. 21 (1979),516.
4.	ipr-mus LD50:105 mg/kg	YAKUD5 Gekkan Yakuji. Pharmaceuticals Monthly. 21 (1979),516.

Safety Profile

Poison by ingestion and intraperitoneal routes. Experimental reproductive effects. When heated to decomposition it emits toxic fumes of NO_x and Br⁻.

Hazard Codes: Harmful Xn
Risk Statements: 20/21/22
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed.
Safety Statements: 36
S36:Wear suitable protective clothing.
WGK Germany: 3
RTECS: BZ3280000

Specification

Classification Code of Valopride (CAS NO.4093-35-0 ) : Drug / Therapeutic Agent;Reproductive Effect;Tumor data