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Basic Information
CAS No.: 4260-20-2
Name: 4(3H)-Quinazolinone, 3-(2-bromophenyl)-2-methyl-
Article Data: 9
Molecular Structure:
Molecular Structure of 4260-20-2 (4(3H)-Quinazolinone, 3-(2-bromophenyl)-2-methyl-)
Formula: C15H11BrN2O
Molecular Weight: 315.169
Synonyms: 3-<2-Brom-phenyl>-2-methyl-3H-chinazolin-4-on;
PSA: 34.89000
LogP: 3.45660
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Synthetic route

3-(2-bromophenyl)-2-methyl-2,3-dihydroquinazolin-4(1H)-one

4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane at 20℃; for 0.5h; Green chemistry;81%
118-48-9

isatoic anhydride

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Triethyl orthoacetate

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4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
In neat (no solvent) at 120℃; for 4h; Temperature; Green chemistry;70%
...Expand

3-(2-bromophenyl)quinazolin-4(3H)-one

PEG-400

PEG-400

4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
With p-toluenesulfonic acid monohydrate; oxygen at 110℃; Sealed tube; Green chemistry;67%
34489-85-5

2-amino-N-(2-bromophenyl)benzamide

PEG-400

PEG-400

4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
With p-toluenesulfonic acid monohydrate; oxygen at 110℃; Sealed tube; Green chemistry;67%
615-36-1

2-bromoaniline

89-52-1

o-acetylamino-benzoic acid

4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
With phosphorus trichloride In toluene for 3h; Heating;29%
525-76-8

2-methyl-4-oxo-3,1-benzoxazine

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2-bromoaniline

4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
With acetic acid Heating;
118-92-3

anthranilic acid

4-benzylidene-2-phenyl-5-imidazolone-acetic acid (pseudo)halide

4-benzylidene-2-phenyl-5-imidazolone-acetic acid (pseudo)halide

4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: AcOH / Heating
2: AcOH / Heating
View Scheme
34489-84-4

2-Nitro-benzoesaeure-<2-brom-anilid>

4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: ammonium chloride; zinc / tetrahydrofuran; water / 20 °C
2: L-Tartaric acid; N,N'-Dimethylurea / 90 °C / Green chemistry
3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C / Green chemistry
View Scheme
34489-85-5

2-amino-N-(2-bromophenyl)benzamide

4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: L-Tartaric acid; N,N'-Dimethylurea / 90 °C / Green chemistry
2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C / Green chemistry
View Scheme
Multi-step reaction with 2 steps
1: oxygen; p-toluenesulfonic acid monohydrate / water / 110 °C / Sealed tube; Green chemistry
2: oxygen; p-toluenesulfonic acid monohydrate / 110 °C / Sealed tube; Green chemistry
View Scheme
552-16-9

ortho-nitrobenzoic acid

4260-20-2

2-methyl-3-(o-bromophenyl)-4(3H)-quinazolinone

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 0 - 20 °C
2: triethylamine / dichloromethane
3: ammonium chloride; zinc / tetrahydrofuran; water / 20 °C
4: L-Tartaric acid; N,N'-Dimethylurea / 90 °C / Green chemistry
5: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C / Green chemistry
View Scheme
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