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Basic Information
CAS No.: 496-11-7
Name: INDAN
Article Data: 226
Molecular Structure:
Molecular Structure of 496-11-7 (INDAN)
Formula: C9H10
Molecular Weight: 118.178
Synonyms: Indan(8CI);1,2-Hydrindene;2,3-Dihydro-1H-indene;2,3-Dihydroindene;Benzocyclopentane;Hydrindene;Hydrindonaphthene;Indane;NSC 5292;
EINECS: 207-814-7
Density: 0.997 g/cm3
Melting Point: -51 °C(lit.)
Boiling Point: 176.499 °C at 760 mmHg
Flash Point: 50 °C
Solubility: Soluble in ethanol, diethyl ether, chloroform (slightly), and ether. Insoluble in water.
Appearance: colourless to faintly yellow liquid
Hazard Symbols: HarmfulXn, FlammableF
Risk Codes: 10-65
Safety: 23-24/25-62
Transport Information: UN 3295 3/PG 3
PSA: 0.00000
LogP: 2.17530
Synthetic route
95-13-6

1-indene

496-11-7

INDANE

Conditions
ConditionsYield
With hydrogen; lithium aluminium tetrahydride; nickelocene In tetrahydrofuran Ambient temperature; atmospheric pressure;99%
With fac-[Mn(1,2-bis(di-isopropylphosphino)ethane)(CO)3(CH2CH2CH3)]; hydrogen In diethyl ether at 60℃; under 37503.8 Torr; for 24h;99%
With chloro-trimethyl-silane; benzoic acid; sodium iodide In acetonitrile at 75℃; for 16h; Heating;98%
methyltetrahydrofluorene

methyltetrahydrofluorene

95-13-6

1-indene

A

methylfluorene

methylfluorene

B

496-11-7

INDANE

Conditions
ConditionsYield
palladium on activated carbon at 250℃; for 2h;A 96%
B 99%
17057-95-3

1,2,3,4-tetrahydro-9H-fluorene

95-13-6

1-indene

A

86-73-7

9H-fluorene

B

496-11-7

INDANE

Conditions
ConditionsYield
A n/a
B 99%
A n/a
B 97%
A n/a
B 95%
858259-07-1

2,3-dimethyl-1,4,4a,9a-tetrahydro-fluorene

95-13-6

1-indene

A

496-11-7

INDANE

B

4612-63-9

2,3-dimethyl-9H-fluorene

Conditions
ConditionsYield
palladium on activated carbon at 250℃; for 2h;A 97%
B 93%
52652-40-1

1,4,4a,9a-tetrahydro-fluorene

95-13-6

1-indene

A

86-73-7

9H-fluorene

B

496-11-7

INDANE

Conditions
ConditionsYield
palladium on activated carbon at 250℃; for 2h;A 97%
B 88%
at 250℃; for 2h;A 96%
B 95%
palladium on activated carbon at 230 - 250℃; for 2 - 4h;A 91%
B 88%
83-33-0

inden-1-one

496-11-7

INDANE

Conditions
ConditionsYield
With triethylsilane; trifluorormethanesulfonic acid In dichloromethane for 2h; Ambient temperature;96%
With sodium cyanoborohydride at 20℃; for 0.05h;94%
With [(C6H6)(PCy3)(CO)RuH]+*BF4−; hydrogen; phenol In 1,4-dioxane; isopropyl alcohol at 130℃; under 1520.1 Torr; for 16h; Inert atmosphere; Glovebox; Schlenk technique; chemoselective reaction;90%
115227-67-3

1,9-dibromo-2,7-nonadiyne

496-11-7

INDANE

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane Cyclization; dehydrobromination;89%
42918-20-7

1-allyl-2-bromobenzene

280-64-8

9-bora-bicyclo[3.3.1]nonane

496-11-7

INDANE

Conditions
ConditionsYield
With sodium hydroxide; dihydrogen peroxide; cis-dichloro-1,1'-bis(diphenylphosphino)ferrocene palladium(II) In tetrahydrofuran To a soln. of haloalkene is added 9-BBN at 0°C, mixt. is stirred for 5 h at room temp., catalyst and aq. NaOH are added, after refluxing for 14 h, the unreacted borane is oxidized with H2O2 for 1h.; Isolated by chromy. over silica gel with hexane-ether, identified by IR,(1)H NMR, mass spectrometry, elem. anal.;86%
945546-80-5

6-hydroxy-1,2,3,6-tetrahydroindene-3a-carboxylic acid tert-butyl ester

496-11-7

INDANE

Conditions
ConditionsYield
With BiCl3*H2O In water; acetonitrile at 65 - 70℃; for 8h;81%
With bismuth chloride hydrate In water; acetonitrile at 65 - 70℃;
606-23-5

1H-indene-1,3(2H)-dione

496-11-7

INDANE

Conditions
ConditionsYield
With triethylsilane; trifluoroacetic acid at 50℃; for 20h;80%
With ethanol; PdCl2 activated platinum Hydrogenation;
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    Product Name: INDAN Synonyms: 1,2-Hydrindene;1H-Indene, 2,3-dihydro-;2,3-dihydro-1h-inden;2,3-dihydro-inden;2,3-Dihydroindene;Benzocyclopentane;Hydrindonaphthene;Indene, 2,3-dihydro- CAS: 496-11-7 MF: C9H10 MW: 118.18

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    Product name: Hydrindene CAS No.: 496-11-7 Molecule Formula:C9H10 Molecule Weight:118.18 Purity: 98.0% Package: 200kg/drum Description:Colorless lquid Manufacture Standards:Enterprise Standard TESTING ITEMS SPECIF

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    INDAN Chemical Properties Melting point -51 °C (lit.) Boiling point 176 °C (lit.) density 0.965 g/mL at 25 °C (lit.) vapor pressure 1.5 at 25 °C (extrapolated, Ambrose and Sprake, 1975) refractive index n20/D 1.537

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Chemistry

Indan is also named as 1,2-Hydrindene;1H-Indene, 2,3-dihydro-;2,3-dihydro-1h-inden;2,3-dihydro-inden;2,3-Dihydroindene;Benzocyclopentane;Hydrindonaphthene;indane,and so on.

Molecular Formula: C9H10
Molecular Weight: 118.18
EINECS: 207-814-7
Melting point:  -51 °C(lit.)
Boiling point:  176 °C(lit.)
Density:  0.965 g/mL at 25 °C(lit.)
Refractive index;  n20/D 1.537(lit.)
Flash point:  50 °C 
Storage temp.:  Flammables area
Merck:  14,4931
BRN:  1904376

Uses

Indan is quite commonly used in the synthesis of organic compounds which can be used as drugs,solvents,shock proof agents,solvents,and so on.

Toxicity Data With Reference

1.   

orl-rat LDLo:5000 mg/kg

   28ZRAQ    Toxicology and Biochemistry of Aromatic Hydrocarbons Gerarde, H.,New York, NY.: Elsevier,1960,55.
 
RTECS:  NK3750000

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Mildly toxic by ingestion. When heated to decomposition it emits acrid smoke and fumes.

Hazard Codes:  Xn,F
Risk Statements:  10-65
Safety Statements:  23-24/25-62
RIDADR:  UN 3295 3/PG 3
WGK Germany:  3
Hazard Note:  Flammable
HazardClass:  3
PackingGroup:  III