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| CAS No.: | 58698-89-8 |
|---|---|
| Name: | 3-isothiocyanatopropyltriethoxysilane |
| Article Data: | 8 |
| Molecular Structure: | |
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|
|
| Formula: | C10H21 N O3 S Si |
| Molecular Weight: | 263.433 |
| Synonyms: | 3-(Triethoxysilyl)propylisothiocyanate; Isothiocyanopropyltriethoxysilane;Triethoxy(3-isothiocyanatopropyl)silane |
| Density: | 1g/cm3 |
| Boiling Point: | 290.8°Cat760mmHg |
| Flash Point: | 129.7°C |
| PSA: | 72.14000 |
| LogP: | 2.52770 |
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- 75-15-0
carbon disulfide
- 919-30-2
3-aminopropyltriethoxysilane
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
| Conditions | Yield |
|---|---|
| Stage #1: carbon disulfide; 3-aminopropyltriethoxysilane In tetrahydrofuran at 0 - 5℃; for 3h; Addition; Stage #2: With CYANAMID; triethylamine In tetrahydrofuran at 40℃; for 3h; Elimination; | 95% |
| With sodium In ethanol for 5h; Heating; | 75% |
| Stage #1: carbon disulfide; 3-aminopropyltriethoxysilane In tetrahydrofuran at 0℃; for 3.33333h; Stage #2: With triethylamine; N-Cyanoguanidine In tetrahydrofuran at 40℃; for 3h; | 49% |
| Stage #1: carbon disulfide; 3-aminopropyltriethoxysilane In tetrahydrofuran at 0℃; for 3h; Stage #2: With triethylamine; N-Cyanoguanidine In tetrahydrofuran at 40℃; for 3h; | 49% |
- 463-71-8
thiophosgene
- 919-30-2
3-aminopropyltriethoxysilane
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
| Conditions | Yield |
|---|---|
| Stage #1: 3-aminopropyltriethoxysilane With triethylamine In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere; Stage #2: thiophosgene In tetrahydrofuran at 0℃; for 3h; Inert atmosphere; | 57% |
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
| Conditions | Yield |
|---|---|
| With 1,4-diamino-2,3-dichloroanthraquinone; triethylamine In tetrahydrofuran at 40℃; for 3h; Yield given; |
- 919-30-2
3-aminopropyltriethoxysilane
- 1147550-11-5
ammonium thiocyanate
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
| Conditions | Yield |
|---|---|
| In toluene for 5h; Addition; Heating; |
- 919-30-2
3-aminopropyltriethoxysilane
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: tetrahydrofuran / 3 h / 0 - 5 °C 2: DCDA, Et3N / tetrahydrofuran / 3 h / 40 °C View Scheme |
A
- 34708-08-2
3-triethoxysilylpropyl thiocyanate
B
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
| Conditions | Yield |
|---|---|
| Heating; | A n/a B 1.3 g |
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
- 106-50-3
1,4-phenylenediamine
- 198645-55-5
C6H4(NHC(S)NHCH2CH2CH2Si(OC2H5)3)2
| Conditions | Yield |
|---|---|
| In ethanol for 2h; Heating; | 95% |
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
- 76521-35-2
N-<2-(acetylamino)-2-deoxy-3,4,6-triacetyl-β-D-glucopyranosyl>-N2-<(1,1-dimethylethoxy)carbonyl>-L-asparagine
- 128174-40-3
N4-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-N2-(tert-butoxycarbonyl)-L-asparagine 3-(triethoxysilyl)propylamide
| Conditions | Yield |
|---|---|
| In chloroform for 48h; Ambient temperature; | 88% |
- 35132-20-8
(R,R)-1,2-diphenylethylenediamine
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
| Conditions | Yield |
|---|---|
| In dichloromethane at 25℃; for 24h; Inert atmosphere; | 62% |
- 29841-69-8
(S,S)-1,2-diphenyl-1,2-diaminoethane
- 58698-89-8
triethoxy (3‑isothiocyanatopropyl)silane
| Conditions | Yield |
|---|---|
| In dichloromethane at 25℃; for 24h; Inert atmosphere; | 59% |
- Total:29 Page 1 of 1 1
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