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66648-43-9

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Basic Information
CAS No.: 66648-43-9
Name: N-Trans-Feruloyltyramine
Article Data: 19
Molecular Structure:
Molecular Structure of 66648-43-9 (N-Trans-Feruloyltyramine)
Formula: C18H19NO4
Molecular Weight: 313.353
Synonyms: 6,7-dimethoxy-5-hydroxyflavone;5-hydroxy-6,7-dimethoxy-2-phenyl-4H-1-benzopyran-4-one;6,7-di-O-methyl-baicalein;moupinamide;5-Hydroxy-6,7-dimethoxy-2-phenyl-4H-chromen-4-one;4H-1-Benzopyran-4-one,5-hydroxy-6,7-dimethoxy-2-phenyl;baicalein 6,7-dimethyl ether;N-trans-Feruloyltyramine;Mosloflavone;5-Hydroxy-6,7-dimethoxyflavone;
Density: 1.248g/cm3
Melting Point: 138-140 °C(Solv: chloroform (67-66-3); methanol (67-56-1))
Boiling Point: 603.3°Cat760mmHg
Flash Point: 318.7°C
PSA: 78.79000
LogP: 2.86940
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Synthetic route
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66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
With diethyl cyanophosphonate In N,N-dimethyl-formamide at 0℃; for 6h;80%
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With triethylamine In N,N-dimethyl-formamide at 0℃; for 0.166667h;
Stage #2: tyrosamine With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 20.5h;		73%
Stage #1: (E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 0.5h;
Stage #2: tyrosamine With triethylamine In dichloromethane; N,N-dimethyl-formamide at 20℃; Inert atmosphere;		58%
76733-94-3

N,O-di-(trans-acetylferuloyl)-tyramine

66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
With potassium hydroxide In methanol Ambient temperature;57.5%

Acetic acid 4-{(E)-2-[2-(4-hydroxy-phenyl)-ethylcarbamoyl]-vinyl}-2-methoxy-phenyl ester

66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
With sodium carbonate In ethanol for 2h; Heating; Yield given;
With hydrazine hydrate In acetonitrile at 20℃;0.17 g
51-67-2

tyrosamine

56254-05-8

2,5-dioxopyrrolidin-1-yl (E)-3-(4-hydroxy-3-methoxyphenyl)acrylate

66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; acetone for 24h;
51-67-2

tyrosamine

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caffeic acid coenzyme A thiol ester

66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
With tyramine N-hydroxycinnamoyltransferase; tris hydrochloride In water at 30℃; pH=8.5; Enzyme kinetics; Acylation; Enzymatic reaction;
51-67-2

tyrosamine

30802-00-7, 119785-99-8

4-coumaroyl-coenzyme A

66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
With tyramine N-hydroxycinnamoyltransferase; tris hydrochloride In water at 30℃; pH=8.5; Enzyme kinetics; Acylation; Enzymatic reaction;
51-67-2

tyrosamine

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feruloyl-CoA

66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
With tyramine N-hydroxycinnamoyltransferase; tris hydrochloride In water at 30℃; pH=8.5; Enzyme kinetics; Acylation; Enzymatic reaction;
51-67-2

tyrosamine

54429-80-0

sinapoyl-CoA

66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
With tyramine N-hydroxycinnamoyltransferase; tris hydrochloride In water at 30℃; pH=8.5; Enzyme kinetics; Acylation; Enzymatic reaction;
51-67-2

tyrosamine

66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Et3N / CH2Cl2 / 20 °C
2: 0.17 g / hydrazine monohydrate / acetonitrile / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: tetrahydrofuran / 6 h / Heating
2: 57.5 percent / KOH / methanol / Ambient temperature
View Scheme
50906-12-2

4-acetoxy-3-methoxycinnamoyl chloride

66648-43-9

(E)-N-feruloyltyramine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Et3N / CH2Cl2 / 20 °C
2: 0.17 g / hydrazine monohydrate / acetonitrile / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: tetrahydrofuran / 6 h / Heating
2: 57.5 percent / KOH / methanol / Ambient temperature
View Scheme
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