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Detail of "99469-99-5"

  • CAS Number:
  • 99469-99-5
  • Name:

  • 4-Ethoxycarbonyl-3-ethoxyphenyla-cetic acid

  • Superlist Name:
  • 3-Ethoxy-4-ethoxycarbonyl phenylacetic acid
  • Molecular Structure:
  • Formula:
  • C13H16O5
  • Molecular Weight:
  • 252.26
  • Synonyms:
  • 3-Ethoxy-4-(ethoxycarbonyl)benzeneaceticacid;Ethyl 4-carboxymethyl-2-ethoxybenzoate;[3-Ethoxy-4-(ethoxycarbonyl)phenyl]aceticacid;3-Ethoxy-4-ethoxycarbonylphenyl acetic acid;
  • Density:
  • 1.191 g/cm3
  • Melting Point:
  • 78-80 °C
  • Boiling Point:
  • 414.816 °C at 760 mmHg
  • Flash Point:
  • 155.936 °C
  • Appearance:
  • white to pale yellow solid
  • Hazard Symbols:
  • IrritantXi
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CAS No.99469-99-5 3-Ethoxy-4-ethoxycarbonyl phenylacetic acidCompetitive Product

Assay:98%MIN  Appearance:White to Pal...

Product name:3-Ethoxy-4-ethoxycarbonyl phenylacetic acid Usage: Repaglinide intermediate

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CAS No.99469-99-5 3-Ethoxy-4-ethoxycarbonyl phenylacetic acid

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CAS No.99469-99-5 3-Ethoxy-4-ethoxycarbonyl phenylacetic acid

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CAS No.99469-99-5 3-Ethoxy-4-ethoxycarbonyl phenylacetic acid

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CAS No.99469-99-5 3-Ethoxy-4-ethoxycarbonyl phenylacetic acid

Repaglinide intermediate

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CAS No.99469-99-5 3-Ethoxy-4-ethoxycarbonyl phenylacetic acid

intermediate of Repaglinide

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Reference

New solid forms of 2-ethoxy-4-[N-[1-(2-piperidinophenyl)-3-methylbutyl]aminocarbonylmeth yl]benzoic acid, pharmaceuticals containing these forms, and procedure for their preparation
New solid forms of 2-ethoxy-4-[N-[1-(2-piperidinophenyl)-3-methylbutyl]aminocarbonylmeth yl]benzoic acid, pharmaceuticals containing these forms, and procedure for their preparation. Grell, Wolfgang (Thomae, Dr. Karl, G.m.b.H., Fed. Rep. Ger.). Ger. Offen. DE 3522604 A1 8 Jan 1987, 18 pp. Addn. to Ger. Offen. 3,347,565. (Germany) CODEN: GWXXBX. CLASS: ICM: C07D295-12. ICS: A61K031-445. APPLICATION: DE 85-3522604 25 Jun 1985. DOCUMENT TYPE: Patent CA Section: 27 (Heterocyclic Compounds (One Hetero Atom)) Section cross-reference(s): 1, 63 New solid forms of the title compd.In this article, certain chemicals are used. Some of their cas registry numbers are 108157-53-5 and 99469-99-5 (I) were prepd. from 3-methyl-1-(2-piperidinophenyl)butylamine (II) and an acid III (W = CO2H, protected CO2H) or optionally a reactive deriv. prepd. in situ, cleavage of the protecting group, if necessary, and recrystn. of I from EtOH-H2O (to give form B, m. 140-142°) or MeOH, and subsequent drying (to give form C, m. 75-85°), and conversion of the compd. into its salts. I are antidiabetics. A soln. of II in MeCN was successively treated with III (W = EtO2C), PPh3, NEt3, and CCl4 and the mixt. stirred 15 h at room temp. to give 85% I. I in NaOH-EtOH was neutralized with HCl to give form B, which was converted into form C by recrystg. from MeOH and drying the crystd. product over P2O5. I form B, at 0.1 mg/kg in rats, gave 38, 44, 41, and 40% decrease in blood sugar after 1, 2, 3, and 4 h, resp. Tablets were prepd. comprising I 5.0, corn starch 62.0, lactose 48.0, polyvinylpyrrolidone 4.0, and Mg stearate 1.0 mg. .
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