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Cas Database |
| Name |
2-Iodobenzaldehyde |
EINECS | N/A |
| CAS No. | 26260-02-6 | Density | 1.883 g/cm3 |
| PSA | 17.07000 | LogP | 2.10370 |
| Solubility | N/A | Melting Point |
36-39 °C(lit.) |
| Formula | C7H5IO | Boiling Point | 266.3 °C at 760 mmHg |
| Molecular Weight | 232.021 | Flash Point | 114.8 °C |
| Transport Information | N/A | Appearance | white to light beige low melting crystalline |
| Safety | 26-36 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
Benzaldehyde,o-iodo- (6CI,7CI,8CI);2-Iodobenzaldehyde;o-Iodobenzaldehyde; |
Article Data | 133 |
2-Iodobenzaldehyde Synthetic route
- 5159-41-1
2-iodobenzyl alcohol
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| With manganese(IV) oxide In chloroform at 20℃; for 70h; | 99% |
| With 1-methyl-1H-imidazole; tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate; 4,4'-Dimethoxy-2,2'-bipyridin; 9-azabicyclo[3.3.1]nonane N-oxyl; oxygen In acetonitrile at 20℃; for 1h; | 98% |
| With silica gel; pyridinium chlorochromate In dichloromethane at 20℃; Inert atmosphere; | 98% |
- 6630-33-7
ortho-bromobenzaldehyde
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| With copper(l) iodide; Trimethylenediamine; sodium iodide In 1,4-dioxane for 24h; Finkelstein Reaction; Reflux; Inert atmosphere; | 99% |
| Multi-step reaction with 3 steps 1: 83 percent / TsOH / 5 h / Heating 2: 1.) Grignard reagent, 2.) I2 / 1.), 2.) THF 3: 83 percent / aq. HCl / tetrahydrofuran / 20 h / Ambient temperature View Scheme | |
| With copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine In 1,4-dioxane at 120℃; under 1500.15 Torr; for 24h; Reagent/catalyst; Finkelstein Reaction; Autoclave; Inert atmosphere; Schlenk technique; |
- 80953-51-1
(2-iodophenyl)methyl acetate
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| With methanol; potassium permanganate In ethyl acetate at 25℃; for 14h; | 98% |
| Multi-step reaction with 2 steps 1: aqueous KOH 2: AgNO3; Na2S2O8; water View Scheme |
- 35822-58-3
2-bromobenzaldehyde diethyl acetal
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| Stage #1: 2-bromobenzaldehyde diethyl acetal With n-butyllithium In tetrahydrofuran; hexane at -78 - -10℃; for 1.41667h; Stage #2: With iodine In tetrahydrofuran; hexane at -78 - 20℃; for 12.6667h; | 98% |
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| With Iodine monochloride In dichloromethane at 20℃; for 2h; Inert atmosphere; | 94% |
- 88-67-5
2-Iodobenzoic acid
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| With manganese(IV) oxide; borane-THF Inert atmosphere; | 90% |
| Multi-step reaction with 2 steps 1: 40 percent / HCl / 30 h / Heating 2: 34 percent / diisobutylaluminum hydride / toluene / 2 h / -60 °C View Scheme | |
| Multi-step reaction with 2 steps 1: 67 percent / SOCl2, DMF / 2 h / Heating 2: tert-butyl alcohol, LiAlH4 / bis-(2-methoxy-ethyl) ether / -78 - 20 °C View Scheme |
- 7022-46-0
2-Iodo-N-methyl-N-phenylbenzamide
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| With zirconocene dichloride; lithium tri-t-butoxyaluminum hydride In tetrahydrofuran at 20℃; for 0.116667h; Inert atmosphere; | 90% |
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| With Iodine monochloride In dichloromethane at 20℃; for 2h; Inert atmosphere; | 90% |
| Multi-step reaction with 2 steps 1: acetonitrile / 10 h / 20 °C / pH 5 2: Iodine monochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme |
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| With Iodine monochloride In dichloromethane at 20℃; for 2h; Inert atmosphere; | 89% |
- 26260-02-6
2-iodobenzaldehyde
| Conditions | Yield |
|---|---|
| With Iodine monochloride In dichloromethane at 20℃; for 2h; Inert atmosphere; | 85% |
| Multi-step reaction with 2 steps 1: acetonitrile / 10 h / 20 °C / pH 5 2: Iodine monochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme |
2-Iodobenzaldehyde Chemical Properties
Molecular Formula: C7H5IO
Molar mass: 232.02 g/mol
Density: 1.883 g/cm3
Flash Point: 114.8 °C
Index of Refraction: 1.668
Melting point: 36-39 °C(lit.)
Sensitive: Light Sensitive
Boiling Point: 266.3 °C at 760 mmHg
Vapour Pressure: 0.00873 mmHg at 25°C
Appearance: White to light beige low melting crystalline
Structure of 2-Iodobenzaldehyde (26260-02-6) :
Product Categories of 2-Methyl-3-nitropyridine hydrochloride (63585-69-3) : Aldehydes;Benzaldehyde;Carbonyl Compounds;Iodine Compounds;Phenyls & Phenyl-Het;Aromatic Aldehydes & Derivatives (substituted);Adehydes, Acetals & Ketones
2-Iodobenzaldehyde Toxicity Data With Reference
Carcinogenicity of 2-Iodobenzaldehyde (26260-02-6) hasn't been listed as a carcinogen by NTP, IARC,ACGIH, or CA Prop 65. And its toxicological properties have not been fully investigated.
2-Iodobenzaldehyde Safety Profile
Hazard Codes:Xi.gif){kind=small}
Risk Statements:
36: Irritating to the eyes
37: Irritating to the respiratory system
38: Irritating to the skin
Safety Statements:
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
37: Wear suitable gloves
39: Wear eye/face protection
2-Iodobenzaldehyde Specification
2-Iodobenzaldehyde (26260-02-6) is a compound which also can be called for benzaldehyde, 2-iodo- . 2-Iodobenzaldehyde (26260-02-6) is hazardous,so the first aid measures and others should be known .Such as: When on the skin: first,should flush skin with plenty of water immediatelyfor at least 15 minutes while removing contaminated clothing.Secondly,Get shoesmedical aid . Or in the eyes: Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids.Then get medical aid soon.While ,it's Inhaled: Remove from exposure and move to fresh air immediately.Give artificial respiration While not breathing. when breathing is difficult, give oxygen.And as soon as to get medical aid.Then you have the ingesting of the product : Wash mouth out with water,and get medical aid immediately.Notes to Physician: Treat supportively and symptomatically.
In addition, 2-Iodobenzaldehyde (26260-02-6) can be stable under normal temperature and pressure conditions.It is not compatible with strong oxidizing agents and you must not take it with incompatible materials.And also prevent it to broken down into hazardous decomposition products: carbon dioxide,hydrogen iodide,carbon monoxide.
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