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Cas Database

Name	3-Bromobenzaldehyde	EINECS	221-526-9
CAS No.	3132-99-8	Density	1.577 g/cm³
PSA	17.07000	LogP	2.26160
Solubility	decomposes in water	Melting Point	18-21 °C(lit.)
Formula	C₇H₅BrO	Boiling Point	235.3 °C at 760 mmHg
Molecular Weight	185.02	Flash Point	96.1 °C
Transport Information	N/A	Appearance	clear colorless to yellow liquid after melting
Safety	26-36	Risk Codes	22-36/37/38
Molecular Structure		Hazard Symbols	Xn,Xi
Synonyms	NSC 66828;m-Bromobenzaldehyde;Benzaldehyde,m-bromo- (6CI,7CI,8CI);3-Formyl-1-bromobenzene;3-Formylbromobenzene;	Article Data	224

3-Bromobenzaldehyde Synthetic route

: 15852-73-0
(3-Bromophenyl)methanol

: 3132-99-8
m-bromobenzoic aldehyde

Conditions

Conditions	Yield
With fluorosulfonyl fluoride; potassium carbonate; dimethyl sulfoxide at 20℃; for 12h; chemoselective reaction;	99%
With N-chloro-N-(benzenesulfonyl)benzenesulfonamide In acetonitrile at 20 - 25℃; for 0.25h; Inert atmosphere; chemoselective reaction;	98%
With tert.-butylhydroperoxide; 2,2′-((1E,1′E)-(1,2-phenylenebis(azanylylidene))bis(methanylylidene))diphenolcopper(II); sodium hydroxide In water; acetonitrile at 20℃;	97%

: 14473-91-7, 20595-41-9, 32862-97-8
3-bromocinnamic acid

: 3132-99-8
m-bromobenzoic aldehyde

Conditions

Conditions	Yield
With aluminum oxide; potassium permanganate In dichloromethane at 20℃;	99%

: 108-36-1
1,3-dibromobenzene

: 68-12-2, 33513-42-7
N,N-dimethyl-formamide

: 3132-99-8
m-bromobenzoic aldehyde

Conditions

Conditions	Yield
Stage #1: 1,3-dibromobenzene With tri-n-butyllithium magnesate complex In toluene at 0℃; for 1.5h; Stage #2: N,N-dimethyl-formamide In toluene at 0℃; for 0.5h; Stage #3: With citric acid at 20℃;	99%
Stage #1: 1,3-dibromobenzene With n-butyllithium; isopropylmagnesium chloride In tetrahydrofuran; hexane at 0 - 5℃; for 1h; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran at 0℃; for 1h; Further stages.;	90%
Stage #1: 1,3-dibromobenzene With n-butyllithium In tetrahydrofuran at -78℃; for 0.583333h; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran at -78 - 20℃; for 1.5h;	63.21%

: 62247-78-3
1-bromo-3-(dibromomethyl)benzene

: 3132-99-8
m-bromobenzoic aldehyde

Conditions

Conditions	Yield
With dimethyl sulfoxide at 120℃; for 1h;	95%
With potassium carbonate In dimethylsulfoxide-d6 at 60℃; for 24h; Kinetics; Hydrolysis;

: 75148-49-1
3-bromobenzaldehyde diethylacetal

: 3132-99-8
m-bromobenzoic aldehyde

Conditions

Conditions	Yield
With iron(III) p-toluenesulfonate hexahydrate In water for 1h; Reflux;	95%
bismuth(III) iodide In water at 20℃; for 20h;	89%
With copper(II) sulfate; sodium iodide In acetone at 56℃; for 0.75h;	77%

: 62247-78-3
1-bromo-3-(dibromomethyl)benzene

: 67-68-5
dimethyl sulfoxide

: 3132-99-8
m-bromobenzoic aldehyde

Conditions

Conditions	Yield
at 120℃; for 1h;	95%

: 100-52-7
benzaldehyde

A: 3132-99-8
m-bromobenzoic aldehyde

B: 74553-29-0
2,5-dibromobenzaldehyde

Conditions

Conditions	Yield
With bromine fluoride In ethanol; chloroform at -40℃; for 0.0833333h;	A 94% B 5%
With bromine fluoride In ethanol; chloroform at -40℃; for 0.833333h;	A 5% B 90%

: 82436-20-2
2-(3-bromophenyl)-1,3-dithiolane

: 3132-99-8
m-bromobenzoic aldehyde

Conditions

Conditions	Yield
With silica gel; ferric nitrate In hexane at 50℃; for 0.166667h;	94%

: 50793-32-3
C6H4(3-Br)(CHSCH2CH2CH2S-cyclic)

: 3132-99-8
m-bromobenzoic aldehyde

Conditions

Conditions	Yield
With silica gel; iodic acid at 20℃; for 0.0125h;	94%
With quinolinium monofluorochromate(VI) In acetonitrile for 2.5h; Heating;	93%
With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide In dichloromethane at 20℃; for 2h;	92%
With 2,6-dicarboxypyridinium chlorochromate In acetonitrile for 1.91667h; Heating;	90%

: 17789-14-9
3-(1,3-dioxolan-2-yl)-phenylbromide

: 3132-99-8
m-bromobenzoic aldehyde

Conditions

Conditions	Yield
With carbon tetrabromide In water; acetonitrile at 45℃; for 2h; sonication;	93%
In(OSO2CF3)3 In acetone at 20℃; for 2.5h;	93%
With copper(II) sulfate; sodium iodide In acetone at 56℃; for 0.666667h;	92%

3-Bromobenzaldehyde Chemical Properties

Product Name: 3-Bromobenzaldehyde
Synonyms: m-bromo-benzaldehyd;nsc66828; 3-bromo-benzaldehyd;AKOS BBS-00003144;Benzaldehyde, m-bromo-;3-BROMOBENZALDEHYDE;AKOS B004042;benzaldehyde,3-bromo-;
The Molecular formula of 3-bromo benzaldehyde(3132-99-8): C₇H₅BrO
The Molecular Weight of 3-bromo benzaldehyde(3132-99-8): 185.02
Molecular Structure :

EINECS: 221-526-9
Melting point: 18-21 °C(lit.)
Boiling point: 233-236 °C(lit.)
density: 1.587 g/mL at 25 °C(lit.)
refractive index: n20/D 1.593(lit.)
Flash point: 96 °C
color: very faintly to deep brownish-yellow
Water Solubility: DECOMPOSES
Sensitive: Air Sensitive

3-Bromobenzaldehyde Safety Profile

The Hazard Codes of 3-bromo benzaldehyde(3132-99-8):

Xn,Xi
The Risk Statements information of 3-bromo benzaldehyde(3132-99-8):
22: Harmful if swallowed
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of 3-bromo benzaldehyde(3132-99-8):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
RIDADR: 2810
WGK Germany: 3
RTECS: CU4820000
F: 10
Hazard Note: Irritant

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