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1-(4-methoxyphenyl)nonane
4-Nonylphenol
Conditions | Yield |
---|---|
With perhydrodibenzo-18-crown-6 In toluene for 3h; Product distribution; Ambient temperature; other solvents, addition of isopropanol, other anisole derivatives; | 100% |
With perhydrodibenzo-18-crown-6; toluene for 3h; Ambient temperature; | 100% |
With hydrogen iodide |
4-nonanoylphenol
4-Nonylphenol
Conditions | Yield |
---|---|
With hydrogenchloride; mercury; zinc In ethanol for 20h; Reduction; Heating; | 83% |
With hydrogenchloride; mercury; zinc | 71% |
With potassium hydroxide; hydrazine hydrate 1.) diethylene glycol, reflux, 1h; 2.) reflux, 1h; Yield given. Multistep reaction; |
4-Nonylphenol
Conditions | Yield |
---|---|
With sulfuric acid; hydrogen; palladium on activated charcoal In ethyl acetate Yield given; |
2,6-dibromononylphenol
4-Nonylphenol
Conditions | Yield |
---|---|
With tritium; palladium on activated charcoal Dehalogenation; |
4-Nonylphenol
Conditions | Yield |
---|---|
With hydrogenchloride; amalgamated zinc; acetic acid |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 37 percent / AlCl3 / 1,1,2,2-tetrachloro-ethane / 6 h / 50 °C 2: 83 percent / Zn(Hg); aq. HCl / ethanol / 20 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 37 percent / AlCl3 / 1,1,2,2-tetrachloro-ethane / 6 h / 50 °C 2: 83 percent / Zn(Hg); aq. HCl / ethanol / 20 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 70 percent / AlCl3 / nitrobenzene / 8 h / Ambient temperature 2: 71 percent / Zn(Hg), HCl View Scheme | |
Multi-step reaction with 2 steps 1: AlCl3 / CH2Cl2 / 1.) 0 deg C, 30 min; 0 deg C, 30 min; 2.) room temperature, overnight 2: 1.) hydrazine hydrate, 2.) KOH / 1.) diethylene glycol, reflux, 1h; 2.) reflux, 1h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 70 percent / AlCl3 / nitrobenzene / 8 h / Ambient temperature 2: 71 percent / Zn(Hg), HCl View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Mg / tetrahydrofuran / 3 h / Ambient temperature 2: H2, cc. sulfuric acid / 5percent Pd-C / ethyl acetate View Scheme |
1. | orl-rat LD50:1620 mg/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) No. PB85-143766 . |