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Cas Database |
| Name |
9-Phenylacridine |
EINECS | 210-020-3 |
| CAS No. | 602-56-2 | Density | 1.181 g/cm3 |
| PSA | 12.89000 | LogP | 5.05500 |
| Solubility | N/A | Melting Point |
184°C |
| Formula | C19H13N | Boiling Point | 411.1 °C at 760 mmHg |
| Molecular Weight | 255.319 | Flash Point | 179.8 °C |
| Transport Information | N/A | Appearance | Yellow Powder |
| Safety | 22-24/25 | Risk Codes | N/A |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
9-Phenylacridine;9PA;NSC 62730; |
Article Data | 63 |
9-Phenylacridine Synthetic route
- 602-56-2
9-phenylacridine
| Conditions | Yield |
|---|---|
| With copper(I) oxide; hypophosphorous acid In dichloromethane; water; acetonitrile at 0 - 20℃; | 100% |
| Conditions | Yield |
|---|---|
| With potassium phosphate In toluene at 100℃; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Time; Temperature; Suzuki-Miyaura Coupling; Schlenk technique; Inert atmosphere; | 99% |
| With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In water; toluene at 40℃; for 3h; | 96.8% |
| With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,2-dimethoxyethane; ethanol; water at 90℃; for 24h; Inert atmosphere; | 87% |
| With palladium(II) acetate bis(diphenylphosphino)ferrocene; sodium carbonate In N,N-dimethyl-formamide at 100 - 110℃; for 16h; Phenylation; | 60% |
| With potassium phosphate; palladium diacetate; tricyclohexylphosphine In water; toluene Reflux; |
- 23699-69-6
phenyl(2-(phenylamino)phenyl)methanone
- 602-56-2
9-phenylacridine
| Conditions | Yield |
|---|---|
| With t-butyl bromide In 2,2,2-trifluoroethanol at 20℃; for 24h; Solvent; Inert atmosphere; | 95% |
| With hydrogen iodide; iodine In methanol for 12h; Irradiation; | 63% |
| With hydrogen iodide; iodine In methanol at 32℃; for 12h; Irradiation; | 63% |
| Conditions | Yield |
|---|---|
| With [2,2]bipyridinyl; methanesulfonic acid; palladium diacetate In water at 100℃; for 24h; | 94% |
| With [2,2]bipyridinyl; methanesulfonic acid; palladium diacetate In water at 100℃; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; | 93% |
| Conditions | Yield |
|---|---|
| Stage #1: (2-aminophenyl)(phenyl)methanone; phenylboronic acid With copper diacetate In 2,2,2-trifluoroethanol at 20℃; for 12h; Stage #2: With t-butyl bromide In 2,2,2-trifluoroethanol at 20℃; for 24h; Reagent/catalyst; Solvent; | 91% |
| With copper(II) bis(trifluoromethanesulfonate) In 1,1,2,2-tetrachloroethane at 100℃; for 14h; Reagent/catalyst; Solvent; Temperature; Sealed tube; | 90% |
- 10537-12-9
9-phenyl-9,10-dihydroacridine
- 602-56-2
9-phenylacridine
| Conditions | Yield |
|---|---|
| With 2,3-dicyano-5,6-dichloro-p-benzoquinone In benzene Heating; | 90% |
| With diphenylzinc In toluene at 130℃; for 20h; | 78% |
| With potassium hydroxide; potassium hexacyanoferrate(III); benzene |
| Conditions | Yield |
|---|---|
| Stage #1: (2-aminophenyl)(phenyl)methanone; potassium phenyltrifluoborate With copper diacetate In 2,2,2-trifluoroethanol at 20℃; for 12h; Stage #2: With t-butyl bromide In 2,2,2-trifluoroethanol at 20℃; for 24h; | 86% |
| Conditions | Yield |
|---|---|
| With 2-aminopyridine; palladium(II) trimethylacetate; oxygen; citric acid In toluene at 110℃; under 760.051 Torr; for 18h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; | 83% |
| With oxygen; tris-(o-tolyl)phosphine; palladium dichloride In toluene; 1,1,2,2-tetrachloroethane at 160℃; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Sealed tube; | 82% |
- 10265-83-5
9-phenyl-1,2,3,4-tetrahydroacridine
- 602-56-2
9-phenylacridine
| Conditions | Yield |
|---|---|
| With 2-aminopyridine; palladium(II) trimethylacetate; oxygen In toluene at 110℃; under 760.051 Torr; for 18h; Reagent/catalyst; regioselective reaction; | 82% |
| With 1,10-Phenanthroline; palladium(II) trifluoroacetate; oxygen In 1-methyl-pyrrolidin-2-one at 100℃; for 6h; | 75% |
| Conditions | Yield |
|---|---|
| With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tricyclohexylphosphine In toluene at 160℃; for 20h; Inert atmosphere; regioselective reaction; | 81% |
9-Phenylacridine Chemical Properties
Product Name: Acridine, 9-phenyl- (CAS NO.602-56-2)
Molecular Formula: C19H13N
Molecular Weight: 255.31g/mol
Mol File: 602-56-2.mol
EINECS: 210-020-3
Melting Point: 184°C
Boiling point: 411.1 °C at 760 mmHg
Flash Point: 179.8 °C
Density: 1.181 g/cm3
Surface Tension: 52.7 dyne/cm
Enthalpy of Vaporization: 63.78 kJ/mol
Vapour Pressure: 1.36E-06 mmHg at 25°C
XLogP3-AA: 5.2
H-Bond Donor: 0
H-Bond Acceptor: 1
Structure Descriptors of Acridine, 9-phenyl- (CAS NO.602-56-2):
IUPAC Name: 9-phenylacridine
Canonical SMILES: C1=CC=C(C=C1)C2=C3C=CC=CC3=NC4=CC=CC=C42
InChI: InChI=1S/C19H13N/c1-2-8-14(9-3-1)19-15-10-4-6-12-17(15)20-18-13-7-5-11-
16(18)19/h1-13H
InChIKey: MTRFEWTWIPAXLG-UHFFFAOYSA-N
Product Categories: Miscellaneous
9-Phenylacridine Safety Profile
Safety Information of Acridine, 9-phenyl- (CAS NO.602-56-2):
Safety Statements: 22-24/25
22: Do not breathe dust
24: Avoid contact with skin
25: Avoid contact with eyes
9-Phenylacridine Specification
Acridine, 9-phenyl- , its CAS NO. is 602-56-2, the synonyms are EINECS 210-020-3 ; 9-Phenylacridine .
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