cas 16709-86-7, VINYL(CHLOROMETHYL)DIMETHYLSILANE | Articles data ｜lookchem

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16709-86-7

Articles about 16709-86-7Total 3 be found

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Free-Radical Cyclization in the Synthesis of a 1-Aza-5-silabicyclononan-9-one, a Silicon-Containing β-Lactam
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Altamura, Maria,Giammaruco, Maria,Taddei, Maurizio,Ulivi, Paola
p. 8403 - 8406
(1995)
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SYNTHESIS AND PROPERTIES OF CARBOFUNCTIONAL ORGANOSILICON COMPOUNDS BASED ON CHLOROMETHYLSILANES
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Sheludyakov, V. D.,Zhun', V. I.,Shumilin, M. I.,Bochkarev, V. N.,Slyusarenko, T. F.
p. 1410 - 1414
(2007/10/02)

AMINOMERCURATION-DEMERCURATION OF DIMETHYL(CHLOROALKYL)ALKENYLSILANES AS A ROUTE TO AZASILACYCLOALKANES
3,3-Dimethyl-1-phenyl-1-aza-3-silacyclopentane and 3,3,5-trimethyl-1-phenyl-1-aza-3-silacyclopentane were obtained by the reaction of dimethyl(chloromethyl)vinylsilane and dimethyl(chloromethyl)allylsilane with aniline in THF in the presence of mercury acetate followed by reduction with sodium borohydride.Aminomercuration-demercuration of dimethyl(3-chloropropyl)vinylsilane and dimethyl(3-chloropropyl)allylsilane results in the corresponding 3-chloropropylphenylaminoalkyl derivatives.Dimethyl(3-chloropropyl)(2-phenylaminopropyl)silane undergoes cyclization under the same reaction conditions giving 2,4,4-trimethyl-1-phenyl-1-aza-4-silacycloheptane in low yield.Competitive nucleophilic substitution of the chloroalkyl group of initial silanes by aniline affords dimethyl(phenylaminoalkyl)alkenylsilanes.
Voronkov, M. G.,Kirpichenko, S. V.,Abrosimova, A. T.,Albanov, A. I.,Keiko, V. V.,Lavrent'yev, V. I.
p. 159 - 168
(2007/10/02)

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Chemical Properties

Boiling Point: 121.5 °C at 760 mmHg
Flash Point:8.3 °C
Density: 0.878 g/cm³
Vapor Pressure: 17.5mmHg at 25°C
Refractive Index: n20/D 1.440(lit.)
Sensitive: Air Sensitive
BRN: 2071374
PSA: 0.00000
LogP: 2.61630

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