Synthesis of vinyl thioethers and bis-thioethenes from calcium carbide and disulfides
Bis-thioethenes and vinyl thioethers were obtained from the reaction of disulfides and calcium carbide in good to high yields using a simple synthetic procedure and common laboratory setup. The tolerance of the reaction was investigated by the examples of aliphatic, aromatic, heteroaromatic and sesquiterpenic substrates.
Rodygin, Konstantin S.,Gyrdymova, Yuliya V.,Zarubaev, Vladimir V.
p. 476 - 478
(2017/10/05)
An efficient metal-free pathway to vinyl thioesters with calcium carbide as the acetylene source
Chemical reactions involving high-pressure acetylene are not easily performed in a standard laboratory setup. The risk of explosion and technical difficulties drastically complicate the equipment and greatly increase the cost. In this study, we propose th
Rodygin, Konstantin S.,Ananikov, Valentine P.
supporting information
p. 482 - 486
(2016/01/30)
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