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2047-89-4

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REACTION OF SPIRO WITH GRIGNARD REAGENTS IN THE PRESENCE OF CUPROUS CHLORIDE
Attack of MeMgI and PhMgBr in toluene on spiro (1) in the presence of Cu2Cl2 gives 2'-substituted spiro in quantitative yields.Also, attack of PhCH2CH2MgBr on 1 in the presence of Cu2Cl2 afforded 2'-phenethyl, 2'-H and 2'-benzyl (or 2'-p-xylyl) derivatives in toluene (or p-xylene) as solvent.
Rodriguez, Gonzalo,Benito, Yolanda,Temprano, Fernando
p. 427 - 428
(1985)
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Chemical Properties

Appearance/Colour :Crystalline powder

Melting Point: 140-142 °C

Boiling Point: 340.4 °C at 760 mmHg

Flash Point:148.3 °C

Density: 1.113 g/cm³

Vapor Pressure: 0.00017mmHg at 25°C

Refractive Index: 1.639

PKA: 17.84±0.20(Predicted)

PSA: 15.79000

LogP: 3.43680

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2047-89-4

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Chemical Properties

Appearance/Colour :Crystalline powder

Melting Point: 140-142 °C

Boiling Point: 340.4 °C at 760 mmHg

Flash Point:148.3 °C

Density: 1.113 g/cm³

Vapor Pressure: 0.00017mmHg at 25°C

Refractive Index: 1.639

PKA: 17.84±0.20(Predicted)

PSA: 15.79000

LogP: 3.43680

Global suppliers and manufacturers of 2047-89-4total 10 suppliers on LookChem

Article Database

2047-89-4

Articles about 2047-89-4Total 1 be found

More Articles about upstream products of 2047-89-4

More Articles about downstream products of 2047-89-4

Chemical Properties

Appearance/Colour :Crystalline powder

Melting Point: 140-142 °C

Boiling Point: 340.4 °C at 760 mmHg

Flash Point:148.3 °C

Density: 1.113 g/cm3

Vapor Pressure: 0.00017mmHg at 25°C

Refractive Index: 1.639

PKA: 17.84±0.20(Predicted)

PSA: 15.79000

LogP: 3.43680

Global suppliers and manufacturers of 2047-89-4total 10 suppliers on LookChem

Density: 1.113 g/cm³