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32833-96-8

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A FACILE, CONVENIENT AND SELECTIVE HOMOLYTIC CARBAMOYLATION OF HETEROAROMATIC BASES
The oxidative decarboxylation of monoamides of oxalic acid provides carbamoyl radicals, which are useful for the selective carbamoylation of protonated heteroaromatic bases; this reaction represents the first general and selective method for the N-alkyl or N-arylcarbamoylation of heteroaromatic bases.Compared to alkoxycarbonylation, this reaction is much more effective and selective, owing to more favourable polar and enthalpic effects.The importance of the steric effects is also emphasized.
Coppa, Fausta,Fontana, Francesca,Lazzarini, Edoardo,Minisci, Francesco
p. 2687 - 2696
(2007/10/02)

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Chemical Properties

Melting Point: 114-118 °C
Boiling Point: 210.8 °C at 760 mmHg
Flash Point:81.3 °C
Density: 1.251 g/cm³
Solubility:soluble in Methanol
Storage Temp.:Sealed in dry,Room Temperature
Vapor Pressure: 0.0748mmHg at 25°C
Refractive Index: 1.465
PKA: 3.13±0.40(Predicted)
PSA: 57.61000
LogP: -0.84080

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