cas 3546-03-0, cyamemazine | Articles data ｜lookchem

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3546-03-0

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N-demethylation of cyamemazine via non-classical Polonovski reaction and its conjugation to bovine serum albumin
A modified Polonovski reaction has been employed to obtain the N-demethylated metabolite of the neuroleptic drug cyamemazine. The synthesis involves N-oxide formation, isolation of the corresponding N-oxide, and a FeSO4·7H2O mediated Polonovski reaction to afford the desired monodesmethyl cyamemazine. In a subsequent step the hapten N-demethylcyamemazine-hemiglutarate was synthesized and its conjugated to bovine serum albumin (BSA).
Singh, Gurmit,Koerner, Terry B.,Godefroy, Samuel Benrejeb,Armand, Claude
p. 2160 - 2162
(2012)
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An improved process for the preparation of pure cyamemazine and salts thereof
The present invention provides an improved process for the preparation of cyamemazine of formula-1 or its pharmaceutically acceptable salt thereof, which is substantially free of impurities.
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(2014/07/09)

Synthesis of deuterium-labeled cyamemazine and monodesmethyl cyamemazine
A novel approach is presented for the synthesis of cyamemazine maleate and N-desmethyl cyamemazine maleate using a 10-(amino-2-methylpropyl)phenothiazine derivative. This method was successfully applied to the synthesis of [ 2H6]cyamemazine maleate and N-desmethyl-[ 2H3]cyamemazine maleate.
Bolla, R. Sekhar,Kasi Viswanath
p. 82 - 85
(2014/03/21)

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Chemical Properties

Melting Point: 90-95°C
Boiling Point: 479 °C at 760 mmHg
Flash Point:243.5 °C
Density: 1.21 g/cm³
Solubility:DMSO: ≥5mg/mL
Storage Temp.:Refrigerator
Vapor Pressure: 2.46E-09mmHg at 25°C
Refractive Index: 1.654
PKA: 9.31±0.28(Predicted)
PSA: 55.57000
LogP: 4.42368

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