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100-77-6

100-77-6

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Relevant articles and documentsAll total 15 Articles be found

4-[(3-chlorophenyl)diazenyl]-2-{[tris(hydroxymethyl)methyl]-aminomethyle ne}cyclohexa-3,5-dien-1(2H)-one

Odabasoglu, Mustafa,Albayrak, Cigdem,Bueyuekguengoer, Orhan,Goesmann, Helmut

, p. o234-o236 (2003)

The title compound, C17H18ClN3O4, adopts the keto-amine tautomeric form and displays an intramolecular N-H...O hydrogen bond [N...O = 2.639 (2) A]. The configuration around the azo N=N double bond is trans, and

TETRAZOLE DERIVATIVES AS MODULATORS OF METABOTROPIC GLUTAMATE RECEPTORS

-

Page/Page column 25, (2008/06/13)

The present invention relates to new compounds of formula (I) wherein Y1 and Y2 selected from the group consisting of hydrogen, halogen atom, C1-4 alkyl, C1-4 alkoxy or cyano group, X is oxygen or two hydrogen a

Synthesis of L-6-chloropyrroloindoline of chloptosin cyclohexapeptide

Kim, Young-Ah,Han, So-Yeop

, p. 2931 - 2943 (2007/10/03)

Chloptosin is an apoptosis-inducing dimeric cyclohexapeptide. Enantio-selective synthesis of L-6-chloropyrroloindoline, as the key chiral synthon of the cyclohexapeptide of chloptosin, was successfully achieved starting from 3-chloroaniline by utilizing F

Process route upstream and downstream products

Process route

3-chloro-aniline
108-42-9

3-chloro-aniline

3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

Conditions
Conditions Yield
With sodium nitrite; In hydrogenchloride; water; at 25 ℃; Rate constant;
With sulfuric acid; nitric acid; arsenic(III) trioxide; Salz entsteht;
With nitric acid; arsenic(III) trioxide; Salz entsteht;
With hydrogenchloride; sodium nitrite; Salz entsteht;
With hydrogenchloride; cis-nitrous acid;
With sodium nitrite;
With hydrogenchloride; sodium nitrite; In water;
With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃;
With hydrogenchloride; sodium nitrite; at 0 - 5 ℃; for 0.166667h;
With hydrogenchloride; sodium nitrite; In water; at 0 ℃;
With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃;
With hydrogenchloride; sodium nitrite; In water; at -0.15 - 4.85 ℃;
With hydrogenchloride; sodium acetate; sodium nitrite; In water; at 0 ℃; for 0.333333h; pH=3 - 4;
With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃; for 0.25h;
With hydrogenchloride; sodium nitrite; In water; at 0 ℃;
C<sub>12</sub>H<sub>10</sub>ClN<sub>3</sub>O

C12H10ClN3O

3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

Conditions
Conditions Yield
With oxalyl dichloride; In toluene; for 0.166667h; Ambient temperature;
83%
3-chloroaniline hydrochloride
141-85-5

3-chloroaniline hydrochloride

3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

Conditions
Conditions Yield
With tert.-butylnitrite; In acetonitrile; at 20 ℃; for 0.166667h;
C<sub>14</sub>H<sub>11</sub>ClN<sub>4</sub>S
78403-06-2

C14H11ClN4S

3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

2-Imino-3-methylbenzthiazolin-hydrochlorid

2-Imino-3-methylbenzthiazolin-hydrochlorid

Conditions
Conditions Yield
With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; Rate constant; Mechanism;
C<sub>14</sub>H<sub>11</sub>ClN<sub>4</sub>S
78381-88-1

C14H11ClN4S

3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

2-Imino-3-methylbenzthiazolin-hydrochlorid

2-Imino-3-methylbenzthiazolin-hydrochlorid

Conditions
Conditions Yield
With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; Rate constant; Mechanism;
isopentyl nitrite
110-46-3

isopentyl nitrite

3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

Conditions
Conditions Yield
With ethanol; Salz entsteht;
isopentyl nitrite
110-46-3

isopentyl nitrite

3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

Conditions
Conditions Yield
With ethanol; Salz entsteht;
3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

3-chlorophenylthiol
2037-31-2

3-chlorophenylthiol

Conditions
Conditions Yield
3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

1,3-Dichlorobenzene
541-73-1

1,3-Dichlorobenzene

Conditions
Conditions Yield
Salz reagiert nach dem Sandmeyerschen Verfahren;
hydrogen iodide
10034-85-2

hydrogen iodide

3-chlorobenzenediazonium chloride
100-77-6

3-chlorobenzenediazonium chloride

3-iodochlorobenzene
625-99-0

3-iodochlorobenzene

Conditions
Conditions Yield
Salz reagiert;

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