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Fmoc-Lys(Trt)-OH is a chemical with a specific purpose. Lookchem provides you with multiple data and supplier information of this chemical.

111061-54-2

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111061-54-2 Usage

Chemical Properties

White to off-white crystals

Check Digit Verification of cas no

The CAS Registry Mumber 111061-54-2 includes 9 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 6 digits, 1,1,1,0,6 and 1 respectively; the second part has 2 digits, 5 and 4 respectively.
Calculate Digit Verification of CAS Registry Number 111061-54:
(8*1)+(7*1)+(6*1)+(5*0)+(4*6)+(3*1)+(2*5)+(1*4)=62
62 % 10 = 2
So 111061-54-2 is a valid CAS Registry Number.

111061-54-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 17, 2017

Revision Date: Aug 17, 2017

1.Identification

1.1 GHS Product identifier

Product name Fmoc-Lys(Trt)-OH

1.2 Other means of identification

Product number -
Other names N|A-Fmoc-N|A-trityl-L-glutamine

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:111061-54-2 SDS

111061-54-2Relevant articles and documents

Preparation method of N epsilon-tert-butoxycarbonyl-N alpha-fluorenylmethoxycarbonyl-N epsilon-methyl-lysine

-

Paragraph 0024; 0025; 0029; 0030, (2018/09/08)

The invention discloses a preparation method of N epsilon-tert-butoxycarbonyl-N alpha-fluorenylmethoxycarbonyl-N epsilon-methyl-lysine. The preparation method comprises the following steps: taking N alpha-fluorenylmethoxycarbonyl-lysine hydrochloride as a raw material, performing alkylation with halide (R-X) under alkaline conditions, performing reductive amination on alkylate in an aqueous formaldehyde solution to introduce methyl, removing an R group of a reductive amination product under acidic conditions, then introducing a t-butyloxycarboryl (BOC) protecting group under alkaline conditions and performing re-crystallization treatment to obtain a product. The preparation method disclosed by the invention is simple in synthetic route and mild in reaction conditions, and the next-step reaction can be directly carried out after an intermediate is simply washed and concentrated. The reaction yield in each step is close to quantification, the total yield can reach above 80 percent, the purity of a final product exceeds 98 percent, and a safe and efficient synthetic route is provided for the preparation of the N epsilon-tert-butoxycarbonyl-N alpha-fluorenylmethoxycarbonyl-N epsilon-methyl-lysine.

Application of the Trt and Fmoc Groups for the Protection of Polyfunctional α-Amino Acids

Barlos, Kleomenis,Mamos, Petros,Papaioannou, Dionysios,Patrianakou, Stella,Sanida, Chariklia,Schaefer, Wolfram

, p. 1025 - 1030 (2007/10/02)

Simple methods for the preparation of ditrityl amino acids 3 and their application for the synthesis of the peptides 9-27 are described.Selective detritylation of 3 and of the synthesized ditrityl peptides is achieved with 1percent trifluoroacetic acid in dichloromethane.The resulting Nα-detritylated amino acids 5 were converted into the corresponding fluorenylmethoxycarbonyl amino acids 6 under Schotten-Baumann conditions using fluorenylmethyl chloroformate.

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