13070-22-9Relevant articles and documents
Synthetic method for N-substituent-3-aminoacrolein
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Paragraph 0027; 0038; 0039; 0040, (2017/08/29)
The invention discloses a synthetic method for N-substituent-3-aminoacrolein. The method comprises the following steps: with secondary amine and 3-chloroallyl alcohol as raw materials, and active manganese dioxide as a catalyst, carrying out introducing into an air environment, then carrying out a reaction at 0.5 to 2.5 MPa and 40 to 90 DEG C for 6 to 14 h, and after completion of the reaction, postprocessing a reaction solution so as to obtain an N-substituent-3-aminoacrolein derivative, wherein the yield is 68% to 97%. Compared with a conventional method for synthesizing the N-substituent-3-aminoacrolein, the method provided by the invention has the advantages of low toxicity, low pollution, simple operation, etc.
REACTION OF TRIMETHYLSILYLPROPYNAL WITH DIALKYLAMINES
Borisova, A. N.,Medvedeva, A. S.,Kalikhman, I. D.,Vyazankin, N. S.
, p. 1730 - 1731 (2007/10/02)
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