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| CAS No.: | 79-40-3 |
|---|---|
| Name: | Dithiooxamide |
| Molecular Structure: | |
|
|
|
| Formula: | C2H4N2S2 |
| Molecular Weight: | 120.199 |
| Synonyms: | Oxamide,dithio- (8CI);Dithiooxalic acid diamide;Ethanedithioamide;Hydrorubeanic acid;NSC 1893;Rubean;Rubeane;Rubeanic acid; |
| EINECS: | 201-203-9 |
| Density: | 1.523 g/cm3 |
| Melting Point: | ≥300 °C(lit.) |
| Boiling Point: | 252.1 °C at 760 mmHg |
| Flash Point: | 106.2 °C |
| Solubility: | Soluble in alcohols. Slightly soluble in water. Insoluble in ether |
| Appearance: | orange to brown crystalline powder |
| Hazard Symbols: |
 Xn
|
| Risk Codes: | 22-36/37/38 |
| Safety: | 36/37 |
| PSA: | 116.22000 |
| LogP: | 0.95920 |
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| Conditions | Yield |
|---|---|
| With Lawessons reagent In acetonitrile Heating; | 67.36% |
| Conditions | Yield |
|---|---|
| With Lawessons reagent In toluene at 80℃; for 0.5h; Other reagent; | A 32% B 14% |
| With tetraphosphorus decasulfide In 1,4-dioxane at 80℃; for 0.2h; other reagent; | A 21% B 14% |
| Conditions | Yield |
|---|---|
| With hydrogen sulfide in alkoh.Loesung; | |
| With sodium hydrogensulfide das Natriumsalz entsteht, in alkoholischer Loesung; | |
| With cyclohexane-1,1-dithiol In ethanol | |
| With hydrogen sulfide in alkoh.Loesung; | |
| With hydrogenchloride; sodium hydrogensulfide; water |
- 64-17-5
ethanol
- 100-63-0
phenylhydrazine
A
- 178168-62-2
amino-(N'-phenyl-hydrazono)-acetonitrile
B
- 7783-06-4
hydrogen sulfide
C
- 79-40-3
dithiooxamide
| Conditions | Yield |
|---|---|
| Kinetics; decomposition in a N2 gas flow; |
| Conditions | Yield |
|---|---|
| In ethanol at 78℃; | 100% |
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Trimethylenediamine
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dithiooxamide
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1,1',4,4',5,5',6,6'-octahydro-2,2'-bipyrimidine
| Conditions | Yield |
|---|---|
| Stage #1: dithiooxamide With ethyl bromide In ethanol at 60℃; for 4h; Inert atmosphere; Schlenk technique; Stage #2: Trimethylenediamine In ethanol at 60 - 80℃; for 1.33333h; Inert atmosphere; Schlenk technique; | 100% |
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Chemistry
Molecular Formula:C2H4N2S2
Molecular Weight:120.20
EINECS:201-203-9
Density:1.523 g/cm3
Melting Point:>300 °C
Boiling Point:252.1 °C at 760 mmHg
Flash Point:106.2 °C
Solubility:negligible
Stability:Stable.
Dithiooxamide's Synonyms: DITHIOOXALAMIDE;DITHIOOXALIC DIAMIDE;DITHIOOXAMIDE;ETHANEDITHIOAMIDE;RUBEANE;RUBEAN-HYDROGEN;RUBEANIC ACID;dithiono-oxalicacidiamide
Uses
Toxicity Data With Reference
| 1. | orl-rat LDLo:500 mg/kg | NCNSA6 National Academy of Sciences, National Research Council, Chemical-Biological Coordination Center, Review. 5 (1953),43. | ||
| 2. | orl-mus LD50:350 mg/kg | FATOAO Farmakologiya i Toksikologiya (Moscow). 28 (1965),230. | ||
| 3. | ipr-mus LD50:100 mg/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) AD277-689 . | ||
| 4. | ivn-mus LD50:56 mg/kg | CSLNX* U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) NX#04475 . |
Consensus Reports
Safety Profile
Poison by ingestion, intraperitoneal, and intravenous routes. When heated to decomposition it emits very toxic fumes of NOx and SOx.
Dithiooxamide's Safety Information
Hazard Codes Xn
Risk Statements 22-36/37/38
Safety Statements 36/37
WGK Germany 3
RTECS RP1575000
HS Code 29309070