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Name	Ethyl 2,6-diaminohexanoate dihydrochloride	EINECS	223-340-3
CAS No.	3844-53-9	Density	g/cm³
PSA	78.34000	LogP	3.01040
Solubility	N/A	Melting Point	~150 °C (dec.)
Formula	C8H18 N2 O2 . 2 Cl H	Boiling Point	261.9 °C at 760 mmHg
Molecular Weight	247.165	Flash Point	97.3 °C
Transport Information	N/A	Appearance	White Powder
Safety	22-24/25	Risk Codes	36/37/38
Molecular Structure		Hazard Symbols	36/37/38:;
Synonyms	L-Lysine,ethyl ester, dihydrochloride (9CI); Lysine, ethyl ester, dihydrochloride, L-(7CI,8CI); Lysine ethyl ester dihydrochloride; NSC 162742	Article Data	5

Ethyl 2,6-diaminohexanoate dihydrochloride Synthetic route

: 64-17-5
ethanol

: 657-27-2, 10098-89-2
L-Lysine hydrochloride

: 3844-53-9
L-lysine ethyl ester dihydrochloride

Conditions

Conditions	Yield
With thionyl chloride Reflux;	87%
With thionyl chloride at -10℃; for 6h; Reflux;	87%
With hydrogenchloride at 70℃; for 5h;

: 64-17-5
ethanol

L-lysine-dihydrochloride: L-lysine-dihydrochloride

: 3844-53-9
L-lysine ethyl ester dihydrochloride

Conditions

Conditions	Yield
With hydrogenchloride

: C11H15N2O5PolS

: 3844-53-9
L-lysine ethyl ester dihydrochloride

: C22H38N4O6Pol2S2

Conditions

Conditions	Yield
Stage #1: C11H15N2O5PolS With benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 3h; Stage #2: L-lysine ethyl ester dihydrochloride With dmap In dichloromethane at 20℃; for 42h;	94%

: 3844-53-9
L-lysine ethyl ester dihydrochloride

: 76-83-5
trityl chloride

: ethyl 2-amino-6-(tritylamino)hexanoate

Conditions

Conditions	Yield
With triethylamine In dichloromethane at 20℃; for 6h;	88.8%

: 1521-38-6
2,3-dimethoxybenzoic acid

: 3844-53-9
L-lysine ethyl ester dihydrochloride

: ethyl N2,N6-bis(2,3-dimethoxybenzoyl)-L-lysinate

Conditions

Conditions	Yield
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere;	85%

: 3844-53-9
L-lysine ethyl ester dihydrochloride

: 552-30-7
trimellitic Anhydride

: 1281900-48-8
C26H22N2O10

Conditions

Conditions	Yield
With pyridine; acetic acid at 20℃; for 6h; Reflux;	79%
With pyridine; acetic acid for 8h; Reflux;

: 16024-56-9
2-(2-methoxyethoxy)acetic acid

: 3844-53-9
L-lysine ethyl ester dihydrochloride

: di-(2-methoxyethoxyacetyl)-L-lysine ethyl ester

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; Cooling with ice;	77.8%

: 3844-53-9
L-lysine ethyl ester dihydrochloride

: 30562-34-6
geldanmycin

: (S)-ethyl 2-amino-6-(((4E,6Z,8S,9S,10E,12S,13R,14S,16R)-9-(carbamoyloxy)-13-hydroxy-8,14-dimethoxy-4,10,12,16-tetramethyl-3,20,22-trioxo-2-azabicyclo[16.3.1]docosa-1(21),4,6,10,18-pentaen-19-yl)amino)hexanoate

Conditions

Conditions	Yield
With triethylamine In tetrahydrofuran; methanol at 60℃;	74.1%

: 3844-53-9
L-lysine ethyl ester dihydrochloride

: 1010-93-1
2-methyl-5-nitroimidazole-1-acetic acid

: ethyl 2,6-bis(2-(2-methyl-5-nitro-1H-imidazol-1-yl)acetamido)hexanoate

Conditions

Conditions	Yield
Stage #1: 2-methyl-5-nitroimidazole-1-acetic acid With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide for 0.25h; Inert atmosphere; Stage #2: L-lysine ethyl ester dihydrochloride With triethylamine In N,N-dimethyl-formamide Inert atmosphere;	69%

: C29H51NO15

: 3844-53-9
L-lysine ethyl ester dihydrochloride

: 870821-07-1
C52H102N2O26

Conditions

Conditions	Yield
With triethylamine In N,N-dimethyl-formamide at 20℃;	66%

Ethyl 2,6-diaminohexanoate dihydrochloride Chemical Properties

Molecular Formula :C₈H₂₀Cl₂N₂O₂
Molecular Weight 247.1
Purity >98.0%
Appearance White powder
Melting point: ~150 °C (dec.)
Storage temp:-20°C
Sensitive Hygroscopic

Ethyl 2,6-diaminohexanoate dihydrochloride Toxicity Data With Reference

H-Lys-OEt-2HCl is irritate to skin and mucous membrane.And H-Lys-OEt-2HCl can induce breathing disorders.

Ethyl 2,6-diaminohexanoate dihydrochloride Safety Profile

Risk Statements 36/37/38
Safety Statements 22-24/25

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