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Cas Database |
| Name |
Flupentiol |
EINECS | 220-304-9 |
| CAS No. | 2709-56-0 | Density | 1.2118 (estimate) |
| PSA | 52.01000 | LogP | 4.47750 |
| Solubility | N/A | Melting Point |
N/A |
| Formula | C23H25F3N2OS | Boiling Point | 554.7±50.0 °C(Predicted) |
| Molecular Weight | 434.526 | Flash Point | 289.3oC |
| Transport Information | UN 2811 6.1/PG 3 | Appearance | white or off-white solid |
| Safety | 36/37/39 | Risk Codes | 20/21/22 |
| Molecular Structure |
|
Hazard Symbols | Xn |
| Synonyms |
1-Piperazineethanol,4-[3-[2-(trifluoromethyl)thioxanthen-9-ylidene]propyl]- (7CI,8CI);2-(Trifluoromethyl)-9-[3-[4-(2-hydroxyethyl)piperazin-1-yl]propylidene]thiaxanthen;2-Trifluoromethyl-9-(3-[4-(2-hydroxyethyl)-1-piperazinyl]propylidene)thioxanthene;4-[3-[2-(Trifluoromethyl)thioxanthen-9-ylidene]propyl]-1-piperazineethanol;Fluanxol;Flupenthixol;Flupentixol;Fluxanxol;LC 44;N 7009;Siplaril; |
Article Data | 4 |
Flupentiol Synthetic route
- 2709-56-0
cis-(Z)-flupenthixol
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: (Z)-flupentixol p-chlorobenzoate dihydrochloride With potassium hydroxide In methanol; water at 55℃; for 1h; Stage #2: In water; toluene at 70℃; Stage #3: With cyclohexane at 60℃; | 70% |
- 103-76-4
1-(2-hydroxyethyl)piperazine
- 28973-34-4
2-trifluoromethyl-9-(2-propenylidene)thioxanthene
A
- 2709-56-0
cis-(Z)-flupenthixol
B
- 53772-85-3
flupenthixol
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 1-(2-hydroxyethyl)piperazine; 2-trifluoromethyl-9-(2-propenylidene)thioxanthene at 100℃; under 0.2 - 1 Torr; for 7h; Stage #2: In water; toluene at 70℃; for 0.25h; Stage #3: With sulfuric acid; ammonia more than 3 stages; |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: n-decanoyl chloride; cis-(Z)-flupenthixol In acetone for 1.5h; Heating / reflux; Stage #2: With hydrogenchloride In ethyl acetate at 5 - 25℃; | 85% |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 4-chloro-benzoyl chloride; cis-(Z)-flupenthixol; flupenthixol In ethyl acetate at 40 - 70℃; for 1h; Stage #2: With hydrogenchloride In water at 40℃; for 0.25h; | A 33% B n/a |
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Flupentiol
