Tetrahedron Letters p. 2150 - 2153 (2008)
Update date:2022-08-03
Topics:
Bailey, Patrick D.
Beard, Mark A.
Dang, Hoa P.T.
Phillips, Theresa R.
Price, Richard A.
Whittaker, James H.
N-Debenzylations using catalytic hydrogenolysis often fail to take place unless alcoholic solvents are used, but this can lead to N-alkylation as a side reaction; using trifluoroethanol as the solvent overcomes this problem, and leads to highly reliable hydrogenolyses for a wide range of substrates, including the final deprotection step in our total synthesis of (-)-raumacline.
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