Synthesis of aryl [35S]sulfones: Friedel-Crafts sulfonylation of aryl ethers with high specific activity [35S]methanesulfonyl chloride

DOI: 10.1002/jlcr.1300

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Journal of labelled compounds and radiopharmaceuticals p. 347 - 349 (2007)

Update date:2022-08-05

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Authors:

Wallace, Michael A.

Raab, Conrad

Dean, Dennis

Melillo, David

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Article abstract of DOI:10.1002/jlcr.1300

Lewis acid-assisted sulfonylation of anisole with [³⁵S] methanesulfonyl chloride afforded high specific activity aryl [ ³⁵S]sulfones. Demethylation and treatment with triflic anhydride gave the versatile [³⁵S]triflate 1 in

Full text of DOI:10.1002/jlcr.1300

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