Journal of Organometallic Chemistry p. 267 - 272 (1987)
Update date:2022-08-03
Topics:
Zeldin, Martel
Xu, Jian-Min
2-Fluoro-3-dimethylchlorosilylpyridine (A) and 3-fluoro-4-dimethylchlorosilylpyridine (B) were synthesized from the corresponding fluoro-lithio-pyridines and dimethyldichlorosilane at -76°C. The liquid products were unstable on standing. A and B were hydrolyzed in aqueous ammonia at room temperature to give disiloxanes which are stable crystalline solids. The new compounds were characterized by IR, 1H NMR and MS.
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(2008)Doi:10.1021/ja01527a075
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(1987)Doi:10.1039/c5cc00261c
(2015)Doi:10.1021/jo00131a018
(1995)Doi:10.1016/S0040-4020(01)82072-X
(1986)
