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Facile preparation of a 4-substituted [2,6-14C]pyridine: Synthesis of [14C]SK and F 105809

DOI: 10.1002/(SICI)1099-1344(199608)38:8<761::AID-JLCR887>3.0.CO;2-2

Source and publish data:

Journal of labelled compounds and radiopharmaceuticals p. 761 - 769 (1996)

Update date:2022-09-26

Topics:

Authors:

Heys, J. RichardHeys, J. Richard

VillaniVillani

MastrocolaMastrocola

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Article abstract of DOI:10.1002/(SICI)1099-1344(199608)38:8<761::AID-JLCR887>3.0.CO;2-2

[14C]Formaldehyde was used in a nucleophile-assisted iminium ion cyclization with N-benzyl-3-butynylamine to provide N-benzyl-4-iodo-1,2,5,6-tetrahydro[2, 6-14C2]pyridine. Palladium-catalyzed coupling of this vinyl iodide

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Full text of DOI:10.1002/(SICI)1099-1344(199608)38:8<761::AID-JLCR887>3.0.CO;2-2

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