Tetrahedron p. 123 - 130 (1987)
Update date:2022-08-03
Topics:
Strijtveen, Bert
Feringa, Ben L.
Kellogg, Richard M.
Methylphosphonic dichloride, CH3P(=O)Cl2, reacts cleanly and quantitatively with thiols to form dialkylthiophosphonates, CH3P(=O)(SR)2.From the ratio of the integrations of the 31P absorptions in the NMR spectra, the enantiomeric excesses of the thiols ca
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