Simple Procedures for the Hydrolysis of Trimethyl Trithioorthocarboxylates to Methyl Thiolcarboxylates. A Convenient Route to Electron-Rich Aromatic and Heteroaromatic Methyl Thiolcarboxylates

DOI: 10.1055/s-1988-27548

Source and publish data:

Synthesis p. 300 - 302 (1988)

Update date:2022-08-05

Topics: Hydrolysis Heteroaromatic Aromatic

Authors:

Barbero, Margherita

Cadamuro, Silvano

Degani, Iacopo

Fochi, Rita

Gatti, Antonella

Regondi, Valeria

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Article abstract of DOI:10.1055/s-1988-27548

Trimethyl trithioorthocarboxylates of N,N-dialkylarylamines, pyrroles and indoles were easily converted into the corresponding methyl thiolcarboxylates by partial hydrolysis with DMSO/water (4:1), at 130 deg C for 5-100 h or with DMSO/35percent aqueous te

Full text of DOI:10.1055/s-1988-27548

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