Bulletin of the Chemical Society of Japan p. 423 - 430 (1988)
Update date:2022-08-05
Topics: Synthesis Oxidation Regioselectivity Column chromatography Yield Nucleophile reflux Reduction Recrystallization Mass spectrometry (MS) TLC (thin-layer chromatography) Tautomerism Conjugation Aromaticity Electrophilic Substitution Heterocyclic compound Solvent extraction NMR spectroscopy (Nuclear Magnetic Resonance) Melting Point Determination
Noguchi, Michihiko
Yamamoto, Takashi
Kajigaeshi, Shoji
Saito, Keiji
Arai, Tsuyoshi
3-Phenyl-4H-benzopyrrolo<2,1,5-cd>indolizin-4-one (5) was prepared by saponification accompanied by the decarboxylation of the corresponding 1,2-bis(methoxycarbonyl)derivative, which was obtained by the DDQ oxidation of 5,6-dihydro one.Investigations
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