Chemistry Letters p. 678 - 679 (2011)
Update date:2022-08-02
Topics:
Saito, Kodai
Saigusa, Yoshihiro
Nokami, Toshiki
Yoshida, Jun-Ichi
Electrochemically generated ArS(ArSSAr)+ was found to be an effective activator for glycosylation of thioglycosides. Efficiency of the reaction strongly depends on the nature of the counter anion, and B(C 6F5)4- was the most effective among those examined. The method was applicable to various glyocosyl donors including thiogalactosides and thiomannosides and various acceptors including those having secondary hydroxy groups.
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