Tetrahedron Letters p. 591 - 594 (1992)
Update date:2022-08-02
Topics:
Gupta, Varsha
Kahne, Daniel
Alkyl iodides are converted to the corresponding hydroxymethyl compounds in good yield by treatment with catalytic triphenylgermane-NaBH3CN-AIBN in benzene-THF under an atmosphhere of CO at high pressure. This methodology is used for the synthesis of an analogue of the B ring of the calicheamicin oligoccharide in which the hydroxylamine at C4 is replaced by a hydroxymethyl group.
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