Synthesis of 2,3,6,7-Tetrahydro- and 2,3,4,5,6,7-Hexahydro-1H-1,4-diazepines via a Tandem Michael-type Addition-Intramolecular Aza-Wittig Sequence

DOI: 10.1039/P19930001061

Source and publish data:

Journal of the Chemical Society. Perkin transactions I p. 1061 - 1064 (1993)

Update date:2022-07-30

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Authors:

Benalil, Aziza

Guerin, Andrea

Carboni, Bertrand

Vaultier, Michel

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Article abstract of DOI:10.1039/P19930001061

Intramolecular aza-Wittig reaction of azides derived from 1,2-amino azides and α,β-unsaturated ketones leads to 2,3,6,7-tetrahydro-1H-1,4-diazepines.Reduction of these compounds with lithium aluminium hydride affords the corresponding saturated heterocycles.

Full text of DOI:10.1039/P19930001061

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