Journal of Organic Chemistry p. 5100 - 5106 (1998)
Update date:2022-08-03
Topics:
Abad, Antonio
Agullo, Consuelo
Arno, Manuel
Cunat, Ana C.
Meseguer, Benjamin
Zaragoza, Ramon J.
An efficient synthesis of stypodiol (1) and its epimer at C-14, epistypodiol (2), was accomplished starting from (S)-(+)-carvone (7). The synthesis of both epimeric compounds proceeds through common intermediates using an IMDA reaction, a sonochemical Barbier reaction, and an acid- catalyzed quinol-tertiary alcohol cyclization as key synthetic steps.
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