Journal of Fluorine Chemistry p. 73 - 78 (1995)
Update date:2022-07-31
Topics: Oxidation Fluorination Column chromatography Yield Catalyst Solvent reflux Reduction Recrystallization Nucleophilic substitution Stirring Thiol TLC (thin-layer chromatography) NMR (nuclear magnetic resonance) Vacuum distillation Aryl group Anhydrous conditions Workup Disulfide Alkyl group Electrophilic Substitution Reaction flask GC-MS (Gas Chromatography-Mass Spectrometry)
Ward, Wayne E.
Sicree, Stephen
Chen, Brian
Tamborski, Christ
Syntheses of RC6F4SR' compounds (where R = F, C6H5, H, R' = alkyl, trifluorovinyl) have been accomplished through reaction between ArfSM (where M = Cu, MgX) and an alkyl or trifluorovinyl halide in dimethylacetamide solvent.Minor by-products from competing reactions have been partially characterized by GC-MS analysis. - Keywords: Synthesis; Polyfluoroalkyl sulfides; NMR spectroscopy; Mass spectrometry
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