Chemical Communications p. 1357 - 1360 (2020)
Update date:2022-08-04
Topics:
Ou, Yingcong
Huang, Yuanting
He, Zhenlin
Yu, Guodian
Huo, Yanping
Li, Xianwei
Gao, Yang
Chen, Qian
A phosphoryl radical-initiated Atherton-Todd-type reaction using air as the radical initiator and CHCl3 as the halogenating reagent for the phosphorylation of alcohols, phenols, and amines has been developed. This novel transformation provides a highly efficient route to important phosphinates, phosphinic amides, and phosphoramidates in up to 99% yield with a broad substrate scope under very mild conditions (48 examples).
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