Paper
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Scheme 1 (a) Protonation and (b) schematic adsorption model of the
triazole 1c on API 5L X70 surface in 1 M HCl.
1b). In this case, both models can help to explain the behaviour
of triazoles as corrosion inhibitors.
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6 (a) A. Espinoza-Vazquez, F. J. Rodriguez-Gomez, R. Gonzalez-
4. Conclusions
Olvera, D. Angeles-Beltran, D. Mendoza-Espinosa and
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G. E. Negron-Silva, RSC Adv., 2016, 18, 72885; (b)
The synthesis of 1,2,3-triazoles is usually performed in the
presence of Cu(I) and Cu(II) salts. However, in this study, we
demonstrated that a solid catalytic material such as a Mg(II)/
Fe(III) hydrotalcite and its mixed oxides can catalyse the Huisgen
cycloaddition with good yields. Aer the catalytic process, it is
possible to recover the heterogeneous catalyst for reuse in two
additional reaction cycles with the same efficiency.
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A. Espinoza-Vazquez, G. E. Negron-Silva, R. Gonzalez-
Olvera, D. Angeles-Beltran, M. Romero-Romo and
M. Palomar-Pardave, Arabian J. Sci. Eng., 2017, 42, 163; (c)
A. Espinoza-Vazquez, G. E. Negron-Silva, R. Gonzalez-
Olvera, D. Angeles-Beltran, H. Herrera-Hernandez,
M. A. Romero-Romo and M. E. Palomar-Pardave, Mater.
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Chem. Phys., 2014, 145, 407.
7 For recent reviews about synthesis of 1,2,3-triazole, see:(a)
On the other hand, the 1-benzyl-4-phenyl-1,2,3-triazoles ob-
tained were evaluated as corrosion inhibitors, demonstrating
that the presence of activator groups in the ortho position of one
of the aromatic rings in the inhibitor system inuences the
corrosion inhibition process of API 5L X70 steel submerged in
1 M HCl. The adsorption of the studied compounds, using the
Langmuir equation, reveals that the inhibitor molecule blocks
the active sites by a chemisorption process.
¨
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Acknowledgements
The authors would like to thank Consejo Nacional de Ciencia y
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Tecnologıa (CONACyT project-239938) for nancial support.
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AEV is grateful to DGAPA-UNAM for the Postdoctoral Grant.
FJRG is grateful to FQ-UNAM for the PAIP support. JAMS
acknowledges support by the Royal Society (UK), Newton
Fellowship Alumni program.
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RSC Adv., 2017, 7, 24736–24746 | 24745