Chemistry Letters p. 1645 - 1646 (1983)
Update date:2022-08-11
Topics:
Tobe, Yoshito
Ueda, Ken-ichi
Kakiuchi, Kiyomi
Odaira, Yoshinobu
<6>paracyclophane (1) has been synthesized by oxidative decarboxylation of <6.2.2>propellenecarboxylic acid with lead tetraacetate.Vapor phase thermolysis of 1, affords 3-methylenespiro<5.5>undeca-1,4-diene predominantly, while acid-catalyzed rearrangement of 1 gives the meta and ortho isomers in ratio of 1:3.
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