Journal of Organic Chemistry p. 185 - 189 (1985)
Update date:2022-08-12
Topics:
Pryor, William A.
Gu, Jen-tau
Church, Daniel F.
Free radicals are detected from the ozonation of a series of olefins using a BHT trapping technique.We have determined the structure of the adduct when 3,3-dimethylbutene (tert-butylethylene) is ozonated at -78 deg C and then warmed in the presence of BHT.The adduct can be rationalized as arising from trapping tert-butylperoxyl radicals by BHT to give 2,6-di-tert-butyl-4-(tert-butylperoxy)-4-methyl-2,5-cyclohexadienone (1).
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