Journal of the Chemical Society. Chemical communications p. 99 - 100 (1994)
Update date:2022-08-11
Topics:
Fleming, Ian
Ghosh, Sunil K.
1-Naphth-1-ylethanol 1 of 92percent enantiomeric excess (e.e.) can be raised to 99.6percent e.e. in an overall yield of 78percent by attaching it to oxalyl chloride, separating the lk diester from the ul by crystallisation, and hydrolysing the diester; the method is potentially general for functional molecules that can easily be attached to and then taken off a bifunctional reagent.
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