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631-61-8

Basic Information
CAS No.: 631-61-8
Name: Ammonium acetate
Molecular Structure:
Molecular Structure of 631-61-8 (Ammonium acetate)
Formula: C2H7NO2
Molecular Weight: 77.10
Synonyms: Aceticacid, ammonium salt (8CI,9CI);Aceticacid, ammonium salt (1:1);
EINECS: 211-162-9
Density: 1.07g/mLat 20°C
Melting Point: 110-112 °C (dec.)(lit.)
Boiling Point: 117.1 °C at 760 mmHg
Flash Point: 40 °C
Solubility: 1480 g/L (20 °C) in water
Appearance: white adhering crystals
Hazard Symbols: T
Risk Codes:  F:Highly flammable;
">  F:Highly flammable;
Safety: 24/25
Transport Information: UN 9079
PSA: 40.54000
LogP: 0.41480
Synthetic route
130642-14-7, 130642-18-1

Acetic acid (2R,4R)-2,4-dimethyl-3-nitro-5-oxo-oxazolidin-2-yl ester

A

60-35-5

acetamide

B

631-61-8

ammonium acetate

C

130642-15-8

N-nitroalaninamide

D

515-98-0

Ammonium lactate

E

302-72-7

rac-Ala-OH

Conditions
ConditionsYield
With ammonia In diethyl ether at 25℃; for 0.5h; Mechanism;A n/a
B n/a
C n/a
D n/a
E 60%
108-24-7

acetic anhydride

Millon's base

Millon's base

A

1600-27-7

mercury(II) diacetate

B

631-61-8

ammonium acetate

C

64-19-7

acetic acid

23405-40-5

5-acetylamino-[1,2,4]dithiazole-3-thione

7664-41-7

ammonia

A

631-61-8

ammonium acetate

B

1147550-11-5

ammonium thiocyanate

C

ammonium sulfide

ammonium sulfide

Conditions
ConditionsYield
at 120℃; im Rohr;
60-35-5

acetamide

631-61-8

ammonium acetate

Conditions
ConditionsYield
at 170 - 195℃; Gleichgewicht;
60-35-5

acetamide

concentrated potassium persulfate

concentrated potassium persulfate

A

631-61-8

ammonium acetate

B

64-19-7

acetic acid

67-56-1

methanol

79-20-9

acetic acid methyl ester

7664-41-7

ammonia

A

60-35-5

acetamide

B

631-61-8

ammonium acetate

Conditions
ConditionsYield
at 25℃; Geschwindigkeit;
64-17-5

ethanol

79-20-9

acetic acid methyl ester

7664-41-7

ammonia

A

60-35-5

acetamide

B

631-61-8

ammonium acetate

Conditions
ConditionsYield
at 25℃; Geschwindigkeit;
109-60-4

1-Propyl acetate

aqueous alcoholic NH3

aqueous alcoholic NH3

A

60-35-5

acetamide

B

631-61-8

ammonium acetate

79-20-9

acetic acid methyl ester

7664-41-7

ammonia

aqueous dioxane

aqueous dioxane

A

60-35-5

acetamide

B

631-61-8

ammonium acetate

Conditions
ConditionsYield
at 25℃; Geschwindigkeit;
628-51-3

diacetoxymethane

7664-41-7

ammonia

A

60-35-5

acetamide

B

100-97-0

hexamethylenetetramine

C

631-61-8

ammonium acetate

Conditions
ConditionsYield
in der Kaelte;
16339-12-1

N-nitroso-N,O-dimethylhydroxylamine

64-19-7

acetic acid

platinum

platinum

A

67-56-1

methanol

B

631-61-8

ammonium acetate

C

6998-30-7

methylamine acetate

Conditions
ConditionsYield
Hydrogenation;
3282-32-4

2-diazo-acetophenone

64-19-7

acetic acid

141-78-6

ethyl acetate

palladium

palladium

A

631-61-8

ammonium acetate

B

613-89-8

2-Aminoacetophenone

Conditions
ConditionsYield
Hydrogenation;
56235-95-1

N-nitroso-O,N-diethyl hydroxylamine

64-19-7

acetic acid

platinum

platinum

A

64-17-5

ethanol

B

631-61-8

ammonium acetate

C

ethylamine acetate

ethylamine acetate

Conditions
ConditionsYield
Hydrogenation;

3-acetoxy-2-cyano-3-phenyl-acrylic acid methyl ester

7664-41-7

ammonia

A

60-35-5

acetamide

B

631-61-8

ammonium acetate

C

ammonium compound of benzoylcyanoacetic acid methyl ester

ammonium compound of benzoylcyanoacetic acid methyl ester

D

β-imino-β-phenyl-α-cyano-propionic acid methyl ester

β-imino-β-phenyl-α-cyano-propionic acid methyl ester

glutamic acid (amino acid)

64-19-7

acetic acid

A

56-86-0

L-glutamic acid

B

631-61-8

ammonium acetate

Conditions
ConditionsYield
In water at 16 - 60℃; for 4.3h; Product distribution / selectivity;
2226-88-2

diammonium succinate

64-19-7

acetic acid

A

110-15-6

succinic acid

B

631-61-8

ammonium acetate

Conditions
ConditionsYield
In water at 15 - 140℃; under 50 - 760.051 Torr; for 0.0833333 - 25.33h; Product distribution / selectivity;
at 15 - 85℃; for 2 - 4.5h; Product distribution / selectivity;
2226-88-2

diammonium succinate

64-19-7

acetic acid

A

631-61-8

ammonium acetate

B

38457-08-8

monoammonium succinate

Conditions
ConditionsYield
Product distribution / selectivity;
64-19-7

acetic acid

A

124-04-9

Adipic acid

B

631-61-8

ammonium acetate

Conditions
ConditionsYield
at 15 - 85℃; for 4.5h; Product distribution / selectivity;
68838-35-7, 71411-67-1

octanedioic acid ; acidic ammonium salt

64-19-7

acetic acid

A

505-48-6

octane-1,8-dioic acid

B

631-61-8

ammonium acetate

Conditions
ConditionsYield
at 15℃; for 18h; Product distribution / selectivity;
64-19-7

acetic acid

631-61-8

ammonium acetate

Conditions
ConditionsYield
With ammonia In water
With ammonium hydroxide at 40℃; Concentration; Temperature; Large scale;
53106-52-8

DL-xylose

A

631-61-8

ammonium acetate

B

137296-15-2

L-lactic acid ; ammonium lactate

Conditions
ConditionsYield
With polypeptone; ammonia In water at 37℃; for 25 - 30h; pH=7; Product distribution / selectivity;
7664-41-7

ammonia

64-19-7

acetic acid

631-61-8

ammonium acetate

Conditions
ConditionsYield
for 0.0166667h;

1-[4-amino-3,5-dibromo-N-[(4-oxo-1-piperidinyl)carbonyl]-D-phenylalanyl]-4-(1-methyl-4-piperidinyl)-piperidine

631-61-8

ammonium acetate

1-[4-amino-N-[(4-amino-1-piperidinyl)carbonyl]-3,5-dibromo-D-phenylalanyl]-4-(1-methyl-4-piperidinyl)-piperidine

Conditions
ConditionsYield
Stage #1: 1-[4-amino-3,5-dibromo-N-[(4-oxo-1-piperidinyl)carbonyl]-D-phenylalanyl]-4-(1-methyl-4-piperidinyl)-piperidine; ammonium acetate With sodium cyanoborohydride In methanol at 20℃;
Stage #2: In water
100%
631-61-8

ammonium acetate

100-44-7

benzyl chloride

140-11-4

Benzyl acetate

Conditions
ConditionsYield
In glycerol at 80℃; for 1h; Solvent;100%
In glycerol at 70℃; for 1h;20%
1382354-48-4

1,3-dibutyl-5,6-dimethylbenzimidazolium iodide

631-61-8

ammonium acetate

1382354-56-4

C2H3O2(1-)*C17H27N2(1+)

Conditions
ConditionsYield
Stage #1: ammonium acetate With Amberlyst A-26 (OH- form) In water at 20℃;
Stage #2: 1,3-dibutyl-5,6-dimethylbenzimidazolium iodide In methanol
100%
631-61-8

ammonium acetate

32353-64-3

1-butyl-4-methylpyridin-1-ium iodide

1289675-19-9

1-butyl-4-methylpyridinium acetate

Conditions
ConditionsYield
Stage #1: ammonium acetate With Amberlyst A-26 (OH- form) In water at 20℃;
Stage #2: 1-butyl-4-methylpyridin-1-ium iodide In acetonitrile
100%
631-61-8

ammonium acetate

4333-62-4

1,3-dimethylimidazolim iodide

78643-53-5

1,3-dimethyl-1H-imidazol-3-ium acetate

Conditions
ConditionsYield
Stage #1: ammonium acetate With Amberlyst A-26 (OH- form) In water at 20℃;
Stage #2: 1,3-dimethylimidazolim iodide In methanol
100%
631-61-8

ammonium acetate

65039-05-6

1-methyl-3-(n-butyl)imidazolium iodide

284049-75-8

3-butyl-1-methylimidazolium acetate

Conditions
ConditionsYield
Stage #1: ammonium acetate With Amberlyst A-26 (OH- form) In water at 20℃;
Stage #2: 1-methyl-3-(n-butyl)imidazolium iodide In methanol
100%
631-61-8

ammonium acetate

143085-46-5

1,3-bis(n-butyl)imidazolium iodide

723254-66-8

1,3-dibutylimidazolium acetate

Conditions
ConditionsYield
Stage #1: ammonium acetate With Amberlyst A-26 (OH- form) In water at 20℃;
Stage #2: 1,3-dibutyl-1,3-imidazolium iodide In methanol
100%

3Mg(2+)*Al(3+)*8HO(1-)*0.5CO3(2-)*2H2O

631-61-8

ammonium acetate

Mg3Al(OH)8(AcO)∙2H2O

Conditions
ConditionsYield
In methanol at 25℃; for 1h; Temperature; Time; Solvent; Sonication; Inert atmosphere;100%
631-61-8

ammonium acetate

19132-12-8

1-[(2R,3S,4R,5R)-3,4-dihydroxy-5-(hydroxymethyl)tetrahydrofur-2-yl]-1,4-dihydropyridine-3-carboxamide

nicotinamide riboside acetate salt

Conditions
ConditionsYield
In water at 20℃; for 1h;100%
859213-36-8

(2R,4R)-tert-butyl 2-methyl-4-(tosyloxy)pyrrolidine-1-carboxylate

631-61-8

ammonium acetate

874883-02-0

(2R,4S)-tert-butyl 4-acetoxy-2-methylpyrrolidine-1-carboxylate

Conditions
ConditionsYield
In toluene for 4h; Heating;99%
945244-60-0

1-(benzo[1,3]dioxol-5-yl)-2-(6-ethylpyridin-2-yl)ethane-1,2-dione

51673-84-8

dimethoxyacetaldehyde

631-61-8

ammonium acetate

945244-62-2

4-(benzo[1,3]dioxol-5-yl)-2-(dimethoxymethyl)-5-(6-ethylpyridin-2-yl)-1H-imidazole

Conditions
ConditionsYield
In methanol; water at 20℃; for 3h;99%
631-61-8

ammonium acetate

144486-49-7

[5-Amino-1-(2-hydroxy-ethyl)-1H-imidazol-4-yl]-imino-acetonitrile

1354414-08-6

C2H4O2*C6H11N5O

Conditions
ConditionsYield
In dimethyl sulfoxide at 40℃; for 18h;99%
631-61-8

ammonium acetate

155579-28-5

5-amino-1-(4'-methoxyphenyl)-4-(cyanoformimidoyl)imidazole

1354414-06-4

C2H4O2*C11H13N5O

Conditions
ConditionsYield
In dimethyl sulfoxide at 40℃; for 18h;99%
500-22-1

3-pyridinecarboxaldehyde

65239-07-8

2-(1,3-benzodioxol-5-yl)ethyl isocyanide

631-61-8

ammonium acetate

1357856-68-8

C18H19N3O4

Conditions
ConditionsYield
Stage #1: 3-pyridinecarboxaldehyde; ammonium acetate In trifluoroethanol at 60℃; for 0.5h; Ugi condensation;
Stage #2: 2-(1,3-benzodioxol-5-yl)ethyl isocyanide In trifluoroethanol at 60℃; for 4h; Ugi condensation;
99%
631-61-8

ammonium acetate

123-30-8

4-amino-phenol

104-88-1

4-chlorobenzaldehyde

134-81-6

benzil

1233762-71-4

4-(2-(4-chlorophenyl)-4,5-diphenyl-1H-imidazol-1-yl)phenol

Conditions
ConditionsYield
With Fe-Cu/ZSM-5 In water at 20℃; for 0.0333333h; Sonication;99%
631-61-8

ammonium acetate

104-87-0

4-methyl-benzaldehyde

108-42-9

3-chloro-aniline

134-81-6

benzil

1-(3-chlorophenyl)-4,5-diphenyl-2-p-tolyl-1H-imidazole

Conditions
ConditionsYield
With Fe-Cu/ZSM-5 In water at 20℃; for 0.05h; Sonication;99%
631-61-8

ammonium acetate

123-30-8

4-amino-phenol

100-52-7

benzaldehyde

134-81-6

benzil

4-(2,4,5-triphenyl-1H-imidazol-1-yl)phenol

Conditions
ConditionsYield
With Fe-Cu/ZSM-5 In water at 20℃; for 0.0333333h; Reagent/catalyst; Solvent; Time; Sonication;99%
118-48-9

isatoic anhydride

631-61-8

ammonium acetate

66-77-3

1-naphthaldehyde

31785-60-1

2,3-dihydro-2-(naphthalene-1-yl)quinazolin-4(1H)-one

Conditions
ConditionsYield
With 3,3′-(butane-1,4-diyl)bis(1,2-dimethyl-1H-imidazole-3-ium) dibromide for 0.05h; Microwave irradiation;99%
39516-78-4

4-bromo-2,2,6,6-tetramethyl-3,5-heptanedione

631-61-8

ammonium acetate

144837-00-3

1-[4-(1,1-dimethylethyl)-2-methyl-5-oxazolyl]-2,2-dimethyl-1-propanone

Conditions
ConditionsYield
In acetic acid for 27h; Heating;98%
631-61-8

ammonium acetate

1-butyl-2,3-dimethylimidazolium bromide

945611-41-6

1-(1-butyl)-2,3-dimethylimidazolium acetate

Conditions
ConditionsYield
Stage #1: ammonium acetate With Amberlyst A-26 (OH- form) In water at 20℃;
Stage #2: 1-butyl-2,3-dimethylimidazolium bromide In methanol
98%
118-48-9

isatoic anhydride

631-61-8

ammonium acetate

104-88-1

4-chlorobenzaldehyde

13165-11-2

2-(4-Chloro-phenyl)-2,3-dihydro-1H-quinazolin-4-one

Conditions
ConditionsYield
With 3,3′-(butane-1,4-diyl)bis(1,2-dimethyl-1H-imidazole-3-ium) dibromide for 0.0166667h; Microwave irradiation;98%
With H3PO4/Al2O3 In neat (no solvent) at 100℃; for 0.2h;95%
631-61-8

ammonium acetate

104-87-0

4-methyl-benzaldehyde

106-47-8

4-chloro-aniline

134-81-6

benzil

912952-59-1

1-(4-chlorophenyl)-2-(4-methylphenyl)-4,5-diphenyl-1H-imidazole

Conditions
ConditionsYield
With Fe-Cu/ZSM-5 In water at 20℃; for 0.0333333h; Sonication;98%
631-61-8

ammonium acetate

104-87-0

4-methyl-benzaldehyde

119-53-9

2-hydroxy-2-phenylacetophenone

106-47-8

4-chloro-aniline

912952-59-1

1-(4-chlorophenyl)-2-(4-methylphenyl)-4,5-diphenyl-1H-imidazole

Conditions
ConditionsYield
With Fe-Cu/ZSM-5 In water at 20℃; for 0.0333333h; Sonication;98%
631-61-8

ammonium acetate

104-87-0

4-methyl-benzaldehyde

134-81-6

benzil

371-40-4

4-fluoroaniline

1-(4-fluorophenyl)-4,5-diphenyl-2-p-tolyl-1H-imidazole

Conditions
ConditionsYield
With Fe-Cu/ZSM-5 In water at 20℃; for 0.05h; Sonication;98%
631-61-8

ammonium acetate

104-87-0

4-methyl-benzaldehyde

62-53-3

aniline

134-81-6

benzil

16112-37-1

2-(4-methylphenyl)-1,4,5-triphenyl-1H-imidazole

Conditions
ConditionsYield
With Fe-Cu/ZSM-5 In water at 20℃; for 0.0333333h; Sonication;98%
631-61-8

ammonium acetate

104-87-0

4-methyl-benzaldehyde

134-81-6

benzil

106-40-1

4-bromo-aniline

1332655-57-8

1-(4-bromophenyl)-2-(4-methylphenyl)-4,5-diphenyl-1H-imidazole

Conditions
ConditionsYield
With Fe-Cu/ZSM-5 In water at 20℃; for 0.05h; Sonication;98%
631-61-8

ammonium acetate

100-52-7

benzaldehyde

106-49-0

p-toluidine

134-81-6

benzil

16112-36-0

1-(4-methylphenyl)-2,4,5-triphenyl-1H-imidazole

Conditions
ConditionsYield
With Fe-Cu/ZSM-5 In water at 20℃; for 0.0333333h; Sonication;98%
631-61-8

ammonium acetate

104-87-0

4-methyl-benzaldehyde

82-86-0

acenaphthene quinone

8-(4-methylphenyl)-7H-acenaphtho[1,2-d]imidazole

Conditions
ConditionsYield
With Fe3O4 nanoparticles supported on graphene oxide loaded with C4H8SO3H In ethanol for 0.0833333h; Reflux; Green chemistry;98%
118-48-9

isatoic anhydride

631-61-8

ammonium acetate

1122-91-4

4-bromo-benzaldehyde

2,3-dihydro-2-(4-bromophenyl)quinazolin-4(1H)-one

Conditions
ConditionsYield
With 3,3′-(butane-1,4-diyl)bis(1,2-dimethyl-1H-imidazole-3-ium) dibromide for 0.0166667h; Microwave irradiation;97%
With H3PO4/Al2O3 In neat (no solvent) at 100℃; for 0.283333h;89%
118-48-9

isatoic anhydride

631-61-8

ammonium acetate

99-61-6

3-nitro-benzaldehyde

26029-30-1

2-(4-chlorophenyl)-2,3-dihydroquinazolin-4(1H)-one

Conditions
ConditionsYield
With 3,3′-(butane-1,4-diyl)bis(1,2-dimethyl-1H-imidazole-3-ium) dibromide for 0.0166667h; Microwave irradiation;97%
With H3PO4/Al2O3 In neat (no solvent) at 100℃; for 0.15h;90%
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    Ammonium acetate

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Chemistry

IUPAC Name: Acetic acid; azane
Synonyms of Ammonium acetate (CAS NO.631-61-8): Acetic acid, ammonium salt ; Acetic acid, ammonium salt (1:1)
CAS NO: 631-61-8
Molecular Formula: C2H7NO2
Molecular Weight: 77.08
Molecular Structure:
EINECS: 211-162-9
H bond acceptors: 2
H bond donors: 1
Freely Rotating Bonds: 0
Polar Surface Area: 26.3 Å2
Flash Point: 40 °C
Enthalpy of Vaporization: 23.7 kJ/mol
Boiling Point: 117.1 °C at 760 mmHg
Vapour Pressure: 13.9 mmHg at 25°C 
Melting Point: 110-112 °C (dec.)(lit.)
Storage temp: 2-8°C
Solubility H2O: 1 M at 20 °C, clear, colorless
Sensitive: Hygroscopic
Appearance: white adhering crystals
Product Categories of Ammonium acetate (CAS NO.631-61-8): Pharmaceutical Intermediates;Inorganic Chemicals;ACS GradeSynthetic Reagents;Essential Chemicals;Routine Reagents;Buffers A to ZBiological Buffers;SigmaUltra Buffers;BioUltraProtein Structural Analysis;Molecular Biology;Ammonium Salts;AmmoniumMetal and Ceramic Science;Salts;

Uses

 Ammonium acetate (CAS NO.631-61-8) has a number of distinctive properties since it is the salt of a weak acid and a weak base. Though Ammonium acetate is occasionally employed as a biodegradable de-icing agent, it is often used with acetic acid to create a buffer solution, one that can be thermally decomposed to non-ionic products. Besides, Ammonium acetate also is useful in the Knoevenagel condensation in organic synthesis.
 Ammonium acetate is relatively unusual example of a salt that melts at low temperatures. It can be used with distilled water to make a protein precipitating reagent. And it is often used as an aqueous buffer for ESI mass spectrometry of proteins and other molecules. Because Ammonium acetate is volatile at low pressures, it has been used to replace cell buffers with non-volatile salts, in preparing samples for mass spectrometry.

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
chicken LDLo intraperitoneal 1735mg/kg (1735mg/kg) BEHAVIORAL: ALTERED SLEEP TIME (INCLUDING CHANGE IN RIGHTING REFLEX)

BEHAVIORAL: COMA

LUNGS, THORAX, OR RESPIRATION: DYSPNEA
Biochemical Journal. Vol. 106, Pg. 699, 1968.
mouse LD50 intraperitoneal 736mg/kg (736mg/kg)   French Demande Patent Document. Vol. #2196792,
mouse LDLo intravenous 386mg/kg (386mg/kg)   Journal of Laboratory and Clinical Medicine. Vol. 29, Pg. 809, 1944.
rat LD50 intraperitoneal 632mg/kg (632mg/kg) LUNGS, THORAX, OR RESPIRATION: DYSPNEA

BEHAVIORAL: MUSCLE CONTRACTION OR SPASTICITY)

ENDOCRINE: HYPOGLYCEMIA
Archives of Biochemistry and Biophysics. Vol. 64, Pg. 342, 1956.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Safety Information about Ammonium acetate (CAS NO.631-61-8):
Safety Statements: 24/25
S24/25: Avoid contact with skin and eyes.
RIDADR: UN 9079
WGK Germany: 3
RTECS: AF3675000
F: 3
HS Code: 29152900
Poison by intravenous route. Moderately toxic by intraperitoneal route. When heated to decomposition it emits toxic fumes of NOx and NH3.

Specification

General Information: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approved or equivalent), and full protective gear.
Extinguishing Media: Use water spray, dry chemical, carbon dioxide, or chemical foam.
Handling: Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes. Avoid ingestion and inhalation.
Storage: Store in a cool, dry place. Store in a tightly closed container.