Research on Chemical Intermediates p. 5109 - 5119 (2015)
Update date:2022-08-16
Topics:
Wan, Fuxian
Liu, Mingjie
Zhang, Junzheng
Li, Ying
Jiang, Lin
A novel chelator of 1,4,7,10-tetraazacyclododecane-1,4,7,10-tetraacetic acid (DOTA) functionalized by adamantane was synthesized by nucleophilic substituted reaction of 1,4,7-Tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane (5) and N-(adamantan-1-yl) bromoacetamide (2). The intermediates and target compound (7) were characterized by fourier transform infrared spectroscopy (FT-IR), 1H nuclear magnetic resonance (NMR), 13C NMR, atmospheric-pressure ionization electrospray mass spectrometry (API-ES-MS), and elemental analysis.
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