Journal of the Chemical Society, Dalton Transactions p. 736 - 742 (1980)
Update date:2022-08-28
Topics:
Lewis, Jack
O'Donoghue, Timothy D.
Two quadridentate ligands have been prepared by rection of 2,9-dichloro-1,10-phenantroline with hydrazine hydrate and methylhydrazine.The formation of complexes of AgI, FII, MnII, ZnII, CdII, HgII, and NiII with these ligands is described.Electrical conductivity, i.r., and 1H n.m.r. spectral data of diamagnetic complexes are reported.The compound 2,9-dihydrazino-1,10-phenantroline can also act as a tridentate ligand, as in the complexes with nickel perchlorate, where the metal to ligand ratio is 1 : 2.Electronic spectral data of the nickel(II) complexes are presented.The preparation of a tridentate ligand, 2-(1-methylhydrazino)-1,10-phenantroline, and of nickel(II) and iron(II) complexes of this ligand is also reported.
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